C₄₃H₅₈O₈Si

Base Information

Chemical Name:C₄₃H₅₈O₈Si
CAS No.:1261148-38-2
Molecular Formula:C₄₃H₅₈O₈Si
Molecular Weight:731.014
Hs Code.:

C<sub>43</sub>H<sub>58</sub>O<sub>8</sub>Si

Synonyms:

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Chemical Property of C₄₃H₅₈O₈Si

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Technology Process of C₄₃H₅₈O₈Si

There total 13 articles about C₄₃H₅₈O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1227265-23-7
C₃₁H₃₆O₄Si

: C₄₃H₅₈O₈Si

: 1261148-38-2
C₄₃H₅₈O₈Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: diethyl ether / 1 h / -78 °C / Inert atmosphere

2.1: 20 % Pd(OH)2/C; hydrogen / ethanol; ethyl acetate / 18 h / 25 °C

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 18 h / 25 °C / Inert atmosphere

4.1: dichloromethane / 4 h / 25 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / dichloromethane / 1.5 h / -78 - 25 °C / Inert atmosphere

6.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

7.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (Me₃Sn)2; trifuran-2-yl-phosphane; lithium chloride / tetrahydrofuran / 0.5 h / 25 °C / Inert atmosphere

7.2: 3 h / 40 °C / Inert atmosphere

8.1: Oxone; sodium tetraborate heptahydrate; 1,2:4,5-di(O-i-propylidene)-3-deoxy-3-oxo-β-D-psicopyranose; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; potassium carbonate / Dimethoxymethane; water; acetonitrile / 3 h / 0 °C

With 2,6-dimethylpyridine; Oxone; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trifuran-2-yl-phosphane; [bis(acetoxy)iodo]benzene; 1,2:4,5-di(O-i-propylidene)-3-deoxy-3-oxo-β-D-psicopyranose; sodium tetraborate heptahydrate; 20 % Pd(OH)2/C; (Me₃Sn)2; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; diisobutylaluminium hydride; potassium carbonate; lithium chloride; In tetrahydrofuran; diethyl ether; Dimethoxymethane; ethanol; dichloromethane; water; ethyl acetate; acetonitrile; 1.1: Grignard reaction / 7.2: Stille coupling / 8.1: Shi epoxidation;
DOI:10.1021/ja109531d

Reference yield:

: C₃₀H₄₂O₅Si

: C₄₃H₅₈O₈Si

: 1261148-38-2
C₄₃H₅₈O₈Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (Me₃Sn)2; trifuran-2-yl-phosphane; lithium chloride / tetrahydrofuran / 0.5 h / 25 °C / Inert atmosphere

1.2: 3 h / 40 °C / Inert atmosphere

2.1: Oxone; sodium tetraborate heptahydrate; 1,2:4,5-di(O-i-propylidene)-3-deoxy-3-oxo-β-D-psicopyranose; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; potassium carbonate / Dimethoxymethane; water; acetonitrile / 3 h / 0 °C

With Oxone; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifuran-2-yl-phosphane; 1,2:4,5-di(O-i-propylidene)-3-deoxy-3-oxo-β-D-psicopyranose; sodium tetraborate heptahydrate; (Me₃Sn)2; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; potassium carbonate; lithium chloride; In tetrahydrofuran; Dimethoxymethane; water; acetonitrile; 1.2: Stille coupling / 2.1: Shi epoxidation;
DOI:10.1021/ja109531d

Reference yield:

: C₅H₉IO

: C₄₃H₅₈O₈Si

: 1261148-38-2
C₄₃H₅₈O₈Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: Dess-Martin periodane / dichloromethane / 1.5 h / 25 °C / Inert atmosphere

2.1: dichloromethane / 2 h / 25 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane / 1.5 h / -78 °C / Inert atmosphere

4.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / decane; dichloromethane / 1.5 h / -20 °C / Molecular sieve; Inert atmosphere

5.1: lanthanum(lll) triflate / toluene / 0.33 h / 25 °C / Inert atmosphere

6.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (Me₃Sn)2; trifuran-2-yl-phosphane; lithium chloride / tetrahydrofuran / 0.5 h / 25 °C / Inert atmosphere

6.2: 3 h / 40 °C / Inert atmosphere

7.1: Oxone; sodium tetraborate heptahydrate; 1,2:4,5-di(O-i-propylidene)-3-deoxy-3-oxo-β-D-psicopyranose; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; potassium carbonate / Dimethoxymethane; water; acetonitrile / 3 h / 0 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; Oxone; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifuran-2-yl-phosphane; diethyl (2S,3S)-tartrate; 1,2:4,5-di(O-i-propylidene)-3-deoxy-3-oxo-β-D-psicopyranose; sodium tetraborate heptahydrate; (Me₃Sn)2; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; diisobutylaluminium hydride; potassium carbonate; Dess-Martin periodane; lithium chloride; lanthanum(lll) triflate; In tetrahydrofuran; decane; Dimethoxymethane; dichloromethane; water; toluene; acetonitrile; 2.1: Whiting reaction / 4.1: Sharpless epoxidation / 6.2: Stille coupling / 7.1: Shi epoxidation;
DOI:10.1021/ja109531d