((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (9R,10R)-10-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-9,10-dihydro-benzo[g]chrysen-9-yl ester

Base Information

Chemical Name:((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (9R,10R)-10-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-9,10-dihydro-benzo[g]chrysen-9-yl ester
CAS No.:122048-50-4
Molecular Formula:C₄₆H₅₆O₆
Molecular Weight:704.947
Hs Code.:

((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (9R,10R)-10-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-9,10-dihydro-benzo[g]chrysen-9-yl ester

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Chemical Property of ((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (9R,10R)-10-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-9,10-dihydro-benzo[g]chrysen-9-yl ester

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Technology Process of ((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (9R,10R)-10-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-9,10-dihydro-benzo[g]chrysen-9-yl ester

There total 18 articles about ((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (9R,10R)-10-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-9,10-dihydro-benzo[g]chrysen-9-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 196-78-1
benzo[g]chrycene

: 122048-50-4,122169-07-7
((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (9S,10S)-10-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-9,10-dihydro-benzo[g]chrysen-9-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Na₂Cr₂O₇, glacial acetic acid / 2 h / 90 °C

2: KBH₄ / propan-2-ol; tetrahydrofuran / 3 h / 50 °C

3: 20 mg / pyridine / 16 h / 4 °C

With pyridine; sodium dichromate; potassium borohydride; acetic acid; In tetrahydrofuran; isopropyl alcohol;
DOI:10.1021/jo00276a009

Reference yield:

: 196-78-1
benzo[g]chrycene

: 122048-50-4,122169-07-7
((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (9R,10R)-10-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-9,10-dihydro-benzo[g]chrysen-9-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Na₂Cr₂O₇, glacial acetic acid / 2 h / 90 °C

2: KBH₄ / propan-2-ol; tetrahydrofuran / 3 h / 50 °C

3: 34 mg / pyridine / 16 h / 4 °C

With pyridine; sodium dichromate; potassium borohydride; acetic acid; In tetrahydrofuran; isopropyl alcohol;
DOI:10.1021/jo00276a009

Reference yield:

: 68151-17-7
3,4-dihydrotriphenylen-1(2H)-one

: 122048-50-4,122169-07-7
((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (9S,10S)-10-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-9,10-dihydro-benzo[g]chrysen-9-yl ester

Guidance literature:: Multi-step reaction with 9 steps

1: Zn, I₂ / tetrahydrofuran / 45 °C

2: 1.) p-TsOH, 2.) 10percent KOH / 1.) benzene, RT, overnight, 2.) ethanediol, 185-190 deg C

3: CH₃SO₃H / 4 h / 55 - 60 °C

4: 94 percent / NaBH₄ / tetrahydrofuran; methanol / 1 h / Ambient temperature

5: 100 percent / p-TsOH / benzene / Ambient temperature

6: o-chloranil / benzene / 72 h / Ambient temperature

7: Na₂Cr₂O₇, glacial acetic acid / 2 h / 90 °C

8: KBH₄ / propan-2-ol; tetrahydrofuran / 3 h / 50 °C

9: 20 mg / pyridine / 16 h / 4 °C

With pyridine; potassium hydroxide; sodium tetrahydroborate; o-tetrachloroquinone; sodium dichromate; potassium borohydride; methanesulfonic acid; iodine; toluene-4-sulfonic acid; acetic acid; zinc; In tetrahydrofuran; methanol; isopropyl alcohol; benzene;
DOI:10.1021/jo00276a009