2,6-Dimethyl-5-(2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yl)-4-(2-trifluoromethyl-phenyl)-1,4-dihydro-pyridine-3-carboxylic acid cyclopropylmethyl ester

Base Information

• Chemical Name: 2,6-Dimethyl-5-(2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yl)-4-(2-trifluoromethyl-phenyl)-1,4-dihydro-pyridine-3-carboxylic acid cyclopropylmethyl ester
• CAS No.: 102098-36-2
• Molecular Formula: C₂₂H₂₅F₃NO₅P
• Molecular Weight: 471.413

Synonyms:

Chemical Property of 2,6-Dimethyl-5-(2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yl)-4-(2-trifluoromethyl-phenyl)-1,4-dihydro-pyridine-3-carboxylic acid cyclopropylmethyl ester

Chemical Property:

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Technology Process of 2,6-Dimethyl-5-(2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yl)-4-(2-trifluoromethyl-phenyl)-1,4-dihydro-pyridine-3-carboxylic acid cyclopropylmethyl ester

There total 1 articles about 2,6-Dimethyl-5-(2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yl)-4-(2-trifluoromethyl-phenyl)-1,4-dihydro-pyridine-3-carboxylic acid cyclopropylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

cyclopropylmethyl 3-aminocrotonate (86780-85-0) + (E)-3-(2-Oxo-2λ5-[1,3,2]dioxaphosphinan-2-yl)-4-(2-trifluoromethyl-phenyl)-but-3-en-2-one (115550-23-7) → 2,6-Dimethyl-5-(2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-yl)-4-(2-trifluoromethyl-phenyl)-1,4-dihydro-pyridine-3-carboxylic acid cyclopropylmethyl ester (102098-36-2)

Guidance literature:

In isopropyl alcohol; Heating;

DOI:10.1248/cpb.35.4144

upstream raw materials:

cyclopropylmethyl 3-aminocrotonate

(E)-3-(2-Oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yl)-4-(2-trifluoromethyl-phenyl)-but-3-en-2-one

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