6-deuteriated 1-benzoylnaphthotricyclo-<4.3.0.0^2,9>non-3-ene

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Chemical Name:6-deuteriated 1-benzoylnaphthotricyclo-<4.3.0.0^2,9>non-3-ene
CAS No.:81068-36-2
Molecular Formula:C₂₃H₁₈O
Molecular Weight:311.387
Hs Code.:

6-deuteriated 1-benzoylnaphtho<de-2.3.4>tricyclo-<4.3.0.0<sup>2,9</sup>>non-3-ene

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Chemical Property of 6-deuteriated 1-benzoylnaphthotricyclo-<4.3.0.0^2,9>non-3-ene

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Technology Process of 6-deuteriated 1-benzoylnaphthotricyclo-<4.3.0.0^2,9>non-3-ene

There total 10 articles about 6-deuteriated 1-benzoylnaphthotricyclo-<4.3.0.0^2,9>non-3-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81061-00-9,81130-74-7
rac-8-hydroxyphenyl-9-deuterionaphthobicyclo<3.2.2>nona-2,6,8-triene(1R*)

: 81068-36-2
6-deuteriated 1-benzoylnaphthotricyclo-<4.3.0.0^2,9>non-3-ene

Guidance literature:: Multi-step reaction with 4 steps

1: 2.) pyridinium chlorochromate / 1.) benzophenone / 1.) benzene, irrad., 3 h; 2.) methylene dichloride, 0 deg C, 15 min.

2: benzene / 160 h / 219.9 °C

3: 81 percent / tris(triphenylphosphin)rhodium(I) chloride, H₂ / benzene / 24 h / Ambient temperature; dark

4: benzene / 4 h / Ambient temperature; Irradiation

With Wilkinson's catalyst; hydrogen; pyridinium chlorochromate; benzophenone; In benzene;
DOI:10.1016/S0040-4020(01)92372-5

Reference yield:

: 81061-00-9,81130-74-7
rac-8-hydroxyphenyl-9-deuterionaphthobicyclo<3.2.2>nona-2,6,8-triene(1S*)

: 81068-36-2
6-deuteriated 1-benzoylnaphthotricyclo-<4.3.0.0^2,9>non-3-ene

Guidance literature:: Multi-step reaction with 4 steps

1: 2.) pyridinium chlorochromate / 1.) benzophenone / 1.) benzene, irrad., 3 h; 2.) methylene dichloride, 0 deg C, 15 min.

2: benzene / 160 h / 219.9 °C

3: 81 percent / tris(triphenylphosphin)rhodium(I) chloride, H₂ / benzene / 24 h / Ambient temperature; dark

4: benzene / 4 h / Ambient temperature; Irradiation

With Wilkinson's catalyst; hydrogen; pyridinium chlorochromate; benzophenone; In benzene;
DOI:10.1016/S0040-4020(01)92372-5

Reference yield:

: 208-20-8
pleiadiene

: 81068-36-2
6-deuteriated 1-benzoylnaphthotricyclo-<4.3.0.0^2,9>non-3-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / 24 h / 120 °C

2: 81 percent / tris(triphenylphosphin)rhodium(I) chloride, H₂ / benzene / 24 h / Ambient temperature; dark

3: benzene / 4 h / Ambient temperature; Irradiation

With Wilkinson's catalyst; hydrogen; In benzene;
DOI:10.1016/S0040-4020(01)92372-5