Technology Process of 9Z,11Z,13Z-12-acetoxymethylretinyl acetate
There total 8 articles about 9Z,11Z,13Z-12-acetoxymethylretinyl acetate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 33 percent / LiAlH4 / tetrahydrofuran / 0.5 h / 0 °C
2: Py. / 1 h / Ambient temperature
With
pyridine; lithium aluminium tetrahydride;
In
tetrahydrofuran;
DOI:10.1021/jo00178a014
- Guidance literature:
-
Multi-step reaction with 3 steps
1: aq. HCl / acetone / 1.5 h / Heating
2: 1) KOH / 1) MeOH, 20 deg C, 64 h; 2) Et2O, 20 deg C, 6 h
3: 1) sodium bis<2-methoxyethoxy> aluminohydride; 2) pyridine / 1) toluene, -5 deg C, 0.5 h; 2) Et2O, 35 deg C, 2 h
With
pyridine; hydrogenchloride; potassium hydroxide; sodium bis(2-methoxyethoxy)aluminium dihydride;
In
acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: aq. HCl / acetone / 1.5 h / Heating
2: 1) KOH / 1) MeOH, 20 deg C, 64 h; 2) Et2O, 20 deg C, 6 h
3: 1) sodium bis<2-methoxyethoxy> aluminohydride; 2) pyridine / 1) toluene, -5 deg C, 0.5 h; 2) Et2O, 35 deg C, 2 h
With
pyridine; hydrogenchloride; potassium hydroxide; sodium bis(2-methoxyethoxy)aluminium dihydride;
In
acetone;
