2-phenanthrylacetonitrile

Base Information

• Chemical Name: 2-phenanthrylacetonitrile
• CAS No.: 74676-81-6
• Molecular Formula: C₁₆H₁₁N
• Molecular Weight: 217.27
• Mol file: 74676-81-6.mol

Synonyms:

Chemical Property of 2-phenanthrylacetonitrile

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-phenanthrylacetonitrile

There total 5 articles about 2-phenanthrylacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2-phenanthrylacetamide (10546-36-8) → 2-phenanthrylacetonitrile (74676-81-6)

Guidance literature:

With trichlorophosphate; In N,N-dimethyl-formamide; 1.) 0 deg C, 10 min, 2.) 25 deg C, 20 min, 3.) 100 deg C, 30 min;

Reference yield:

2-phenanthrylmethanol (2606-54-4) → 2-phenanthrylacetonitrile (74676-81-6)

Guidance literature:

Multi-step reaction with 2 steps

1: HBr; benzene

2: ethanolic solution

With hydrogen bromide; benzene;

DOI:10.1021/ja01334a065

Reference yield:

2-(bromomethyl)phenanthrene (2417-66-5) + potassium cyanide (151-50-8) → 2-phenanthrylacetonitrile (74676-81-6)

Guidance literature:

With ethanolic solution;

DOI:10.1021/ja01334a065

upstream raw materials:

2-(bromomethyl)phenanthrene

potassium cyanide

2-phenanthrylacetamide

2-phenanthrylacetic acid