6-Bromo-1-benzoyl-4,5-exo-epoxy-1,2,2a,3,4,5-hexahydrobenzindole

Base Information

Chemical Name:6-Bromo-1-benzoyl-4,5-exo-epoxy-1,2,2a,3,4,5-hexahydrobenzindole
CAS No.:124465-59-4
Molecular Formula:C₁₈H₁₄BrNO₂
Molecular Weight:356.219
Hs Code.:

6-Bromo-1-benzoyl-4,5-exo-epoxy-1,2,2a,3,4,5-hexahydrobenz<c,d>indole

Synonyms:

Suppliers and Price of 6-Bromo-1-benzoyl-4,5-exo-epoxy-1,2,2a,3,4,5-hexahydrobenzindole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-Bromo-1-benzoyl-4,5-exo-epoxy-1,2,2a,3,4,5-hexahydrobenzindole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-Bromo-1-benzoyl-4,5-exo-epoxy-1,2,2a,3,4,5-hexahydrobenzindole

There total 7 articles about 6-Bromo-1-benzoyl-4,5-exo-epoxy-1,2,2a,3,4,5-hexahydrobenzindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 124465-56-1
(6-Bromo-2a,3-dihydro-2H-benzo[cd]indol-1-yl)-phenyl-methanone

: 124465-59-4,124578-79-6
6-Bromo-1-benzoyl-4,5-endo-epoxy-1,2,2a,3,4,5-hexahydrobenzindole

: 124465-59-4,124578-79-6
6-Bromo-1-benzoyl-4,5-exo-epoxy-1,2,2a,3,4,5-hexahydrobenzindole

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 0 ℃; for 36h; Yields of byproduct given;
DOI:10.1016/S0040-4039(00)99288-8

Reference yield: 99.0%

: 124465-56-1
(6-Bromo-2a,3-dihydro-2H-benzo[cd]indol-1-yl)-phenyl-methanone

: 124465-59-4,124578-79-6
6-Bromo-1-benzoyl-4,5-endo-epoxy-1,2,2a,3,4,5-hexahydrobenzindole

: 124465-59-4,124578-79-6
6-Bromo-1-benzoyl-4,5-exo-epoxy-1,2,2a,3,4,5-hexahydrobenzindole

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 0 ℃; for 36h; Yields of byproduct given;
DOI:10.1016/S0040-4039(00)99288-8

Reference yield:

: 65229-90-5
1-benzoyl-1,2,2a,3,4,5-hexahydro-benz[cd]indol-5-ol

: 124465-59-4,124578-79-6
6-Bromo-1-benzoyl-4,5-endo-epoxy-1,2,2a,3,4,5-hexahydrobenzindole

Guidance literature:: Multi-step reaction with 3 steps

1: Br₂/HOAc/NaOAc

3: 1.) NBS, 2.) NaOH / 1.) DMSO, 0.75 h, 23 deg C, 2.) PhCH₃, 30 min, r.t.

With sodium hydroxide; N-Bromosuccinimide; bromine; sodium acetate; acetic acid;
DOI:10.1016/S0040-4039(00)99288-8