lithium diphenyl-2-pyridylmethanethiolate

Base Information

• Chemical Name: lithium diphenyl-2-pyridylmethanethiolate
• CAS No.: 149091-02-1
• Molecular Formula: C₁₈H₁₄NS*Li
• Molecular Weight: 283.323

Synonyms:

Chemical Property of lithium diphenyl-2-pyridylmethanethiolate

Chemical Property:

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Technology Process of lithium diphenyl-2-pyridylmethanethiolate

There total 1 articles about lithium diphenyl-2-pyridylmethanethiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Diphenyl-2-pyridylmethan (3678-70-4) → lithium diphenyl-2-pyridylmethanethiolate (149091-02-1)

Guidance literature:

With n-butyllithium; sulfur; Yield given. Multistep reaction; 1.) THF, hexane, -60 deg C, 2.) THF, hexane, a) -60 deg C, 45 min, b) RT, 1.5 day;

Reference yield: 85.0%

dichloro(1,2-dimethoxyethane)dioxotungsten(VI) (139467-76-8) + lithium diphenyl-2-pyridylmethanethiolate (149091-02-1) → 2[dioxotungsten(VI)[C5H4NCS(Ph)2]2]

Guidance literature:

In tetrahydrofuran; (N2), ligand as suspn in THF slowly treated with metal complex in THF atroom temp., stirred overnight at room temp.; filtered, washed (THF), dried (vac.), elem. anal.;

DOI:10.1039/b006979p

upstream raw materials:

Diphenyl-2-pyridylmethan

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