C₅₈H₅₈N₅O₁₇PS₂

Base Information

Chemical Name:C₅₈H₅₈N₅O₁₇PS₂
CAS No.:202533-77-5
Molecular Formula:C₅₈H₅₈N₅O₁₇PS₂
Molecular Weight:1192.23
Hs Code.:

C<sub>58</sub>H<sub>58</sub>N<sub>5</sub>O<sub>17</sub>PS<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₈H₅₈N₅O₁₇PS₂

Chemical Property:

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Technology Process of C₅₈H₅₈N₅O₁₇PS₂

There total 9 articles about C₅₈H₅₈N₅O₁₇PS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 362-43-6
2',3'-O-isopropylideneuridine

: 202533-77-5
C₅₈H₅₈N₅O₁₇PS₂

Guidance literature:: Multi-step reaction with 8 steps

3: 53 percent / XN₃

4: 1.) PPh₃, 2.) NH₄OH / 1.) pyridine, room temperature, 3 h, 2.) H₂O, 3 h

5: 89 percent / dimethylformamide / 0.02 h

6: 99 percent / pyridine / 12 h / Ambient temperature

7: 96 percent / Bu₄NF*H₂O, AcOH / tetrahydrofuran / 0.67 h / Ambient temperature

8: 2.) DDS, 1H-tetrazole / 1.) pyridine, room temperature, 4 h, 2.) 3.5 h

With 1H-tetrazole; ammonium hydroxide; tetrabutyl ammonium fluoride; acetic acid; triphenylphosphine; dapsone; In tetrahydrofuran; pyridine; N,N-dimethyl-formamide;
DOI:10.1021/jo971797o

Reference yield:

: 89129-13-5
2',3'-O-isopropylidene-5-aminomethyluridine

: 202533-77-5
C₅₈H₅₈N₅O₁₇PS₂

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / dimethylformamide / 0.02 h

2: 99 percent / pyridine / 12 h / Ambient temperature

3: 96 percent / Bu₄NF*H₂O, AcOH / tetrahydrofuran / 0.67 h / Ambient temperature

4: 2.) DDS, 1H-tetrazole / 1.) pyridine, room temperature, 4 h, 2.) 3.5 h

With 1H-tetrazole; tetrabutyl ammonium fluoride; acetic acid; dapsone; In tetrahydrofuran; pyridine; N,N-dimethyl-formamide;
DOI:10.1021/jo971797o

Reference yield:

: 110419-05-1
1-((3aR,4R,6R,6aR)-6-Hydroxymethyl-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-5-piperidin-1-ylmethyl-1H-pyrimidine-2,4-dione

: 202533-77-5
C₅₈H₅₈N₅O₁₇PS₂

Guidance literature:: Multi-step reaction with 7 steps

2: 53 percent / XN₃

3: 1.) PPh₃, 2.) NH₄OH / 1.) pyridine, room temperature, 3 h, 2.) H₂O, 3 h

4: 89 percent / dimethylformamide / 0.02 h

5: 99 percent / pyridine / 12 h / Ambient temperature

6: 96 percent / Bu₄NF*H₂O, AcOH / tetrahydrofuran / 0.67 h / Ambient temperature

7: 2.) DDS, 1H-tetrazole / 1.) pyridine, room temperature, 4 h, 2.) 3.5 h

With 1H-tetrazole; ammonium hydroxide; tetrabutyl ammonium fluoride; acetic acid; triphenylphosphine; dapsone; In tetrahydrofuran; pyridine; N,N-dimethyl-formamide;
DOI:10.1021/jo971797o