2-benzyl-1,2,3,4,7,12-hexahydronaphtho[2,3-h]isoquinoline-7,12-diol

Base Information

• Chemical Name: 2-benzyl-1,2,3,4,7,12-hexahydronaphtho[2,3-h]isoquinoline-7,12-diol
• CAS No.: 80641-40-3
• Molecular Formula: C₂₄H₂₃NO₂
• Molecular Weight: 357.452
• Mol file: 80641-40-3.mol

Synonyms:NSC 373534

Chemical Property of 2-benzyl-1,2,3,4,7,12-hexahydronaphtho[2,3-h]isoquinoline-7,12-diol

Chemical Property:

• Vapor Pressure: 8.74E-14mmHg at 25°C
• Boiling Point: 569°C at 760 mmHg
• Flash Point: 313.2°C
• Density: 1.293g/cm³

Purity/Quality:

98%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-benzyl-1,2,3,4,7,12-hexahydronaphtho[2,3-h]isoquinoline-7,12-diol

There total 1 articles about 2-benzyl-1,2,3,4,7,12-hexahydronaphtho[2,3-h]isoquinoline-7,12-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzoyl-2-aza-1,2,3,4-tetrahydrobenzanthracene-7,12-dione (80641-39-0) → N-benzyl-2-aza-1,2,3,4-tetrahydrobenzanthracene-7,12-diol (80641-40-3)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 18h; Heating;

DOI:10.1021/jo00346a047

Reference yield:

N-benzyl-2-aza-1,2,3,4-tetrahydrobenzanthracene-7,12-diol (80641-40-3) → 2-Azabenzanthracene (25082-33-1)

Guidance literature:

With palladium on activated charcoal; at 200 - 340 ℃; for 2.5h; Yield given;

DOI:10.1021/jo00346a047

upstream raw materials:

N-benzoyl-2-aza-1,2,3,4-tetrahydrobenzanthracene-7,12-dione

Downstream raw materials:

2-Azabenzanthracene

Refernces