Rp-2-((2-methyl-2-hydroxy)ethyl)-1',2',3',4',5'-pentamethylferrocenyl-1-aldehyde

Base Information

• Chemical Name: Rp-2-((2-methyl-2-hydroxy)ethyl)-1',2',3',4',5'-pentamethylferrocenyl-1-aldehyde
• CAS No.: 884010-86-0
• Molecular Formula: C₁₉H₂₆FeO₂
• Molecular Weight: 342.261

Synonyms:

Chemical Property of Rp-2-((2-methyl-2-hydroxy)ethyl)-1',2',3',4',5'-pentamethylferrocenyl-1-aldehyde

Chemical Property:

Purity/Quality:

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Technology Process of Rp-2-((2-methyl-2-hydroxy)ethyl)-1',2',3',4',5'-pentamethylferrocenyl-1-aldehyde

There total 1 articles about Rp-2-((2-methyl-2-hydroxy)ethyl)-1',2',3',4',5'-pentamethylferrocenyl-1-aldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

Rp-(2S,4S)-4-(methoxymethyl)-2-((2-methyl-2-hydroxy)ethyl)-1',2',3',4',5'-pentamethylferrocenyl-1,3-dioxane → Rp-2-((2-propenyl)-1',2',3',4',5'-pentamethylferrocenyl)-1-aldehyde (884010-87-1) + Rp-2-((2-methyl-2-hydroxy)ethyl)-1',2',3',4',5'-pentamethylferrocenyl-1-aldehyde (884010-86-0)

Guidance literature:

With p-toluenesulfonic acid; In dichloromethane; (Ar); Schlenk glassware; mixt. of Fe complex and acid in CH2Cl2 was stirred at ambient temp. for 1-5 h; TLC monitoring; CH2Cl2 added; org. layer washed (satd. aq. NaHCO3, H2O, brine); org. soln. dried (MgSO4); filtered; evapd. (vac.); chromd. (silica);

DOI:10.1016/j.jorganchem.2005.11.051

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