C₂₈H₂₉OP

Base Information

• Chemical Name: C₂₈H₂₉OP
• CAS No.: 1891002-61-1
• Molecular Formula: C₂₈H₂₉OP
• Molecular Weight: 412.511
• Mol file: 1891002-61-1.mol

Synonyms:

Chemical Property of C₂₈H₂₉OP

Chemical Property:

Purity/Quality:

97% purity，>99% ee ^*data from raw suppliers

(2S,3S)-4-(Anthracen-9-yl)-3-(tert-butyl)-2-isopropyl-2,3-dihydrobenzo[d][1,3]oxaphosphole, 97% (>99% ee) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₂₉OP

There total 2 articles about C₂₈H₂₉OP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C28H29O2P → C28H29OP (1891002-61-1)

Guidance literature:

With titanium(IV)isopropoxide; In tetrahydrofuran; for 12h; Inert atmosphere; Reflux;

DOI:10.1002/anie.201600379

Reference yield:

C25H23O2P (1477517-24-0) → C28H29OP (1891002-61-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane / 1 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C

2.1: titanium(IV)isopropoxide / tetrahydrofuran / 12 h / Inert atmosphere; Reflux

With titanium(IV)isopropoxide; lithium diisopropyl amide; In tetrahydrofuran; n-heptane;

DOI:10.1002/anie.201600379

upstream raw materials:

C₂₅H₂₃O₂P