Technology Process of (RS)-2-(3,7-dimethyloctyl)-4'-methoxybenzophenone
There total 8 articles about (RS)-2-(3,7-dimethyloctyl)-4'-methoxybenzophenone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triphenylsilane; di-tert-butyl peroxide / 5 h / 140 °C
1.2: 36 percent / hydrochloric acid / diethyl ether / 70 h
2.1: oxalyl chloride / benzene / 1 h / Heating
3.1: 0.451 g / AlCl3 / 4 h / 140 °C
With
aluminium trichloride; oxalyl dichloride; di-tert-butyl peroxide; HSiPh3;
In
benzene;
3.1: Friedel-Crafts reaction;
DOI:10.1021/jo060481q
- Guidance literature:
-
Multi-step reaction with 2 steps
1: oxalyl chloride / benzene / 1 h / Heating
2: 0.451 g / AlCl3 / 4 h / 140 °C
With
aluminium trichloride; oxalyl dichloride;
In
benzene;
2: Friedel-Crafts reaction;
DOI:10.1021/jo060481q
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: H2
2.1: sodium iodide / acetone / 1 h / Heating
3.1: magnesium / diethyl ether / 20 °C
3.2: 50 percent / diethyl ether; tetrahydrofuran / 3 h / 20 °C
4.1: triphenylsilane; di-tert-butyl peroxide / 5 h / 140 °C
4.2: 36 percent / hydrochloric acid / diethyl ether / 70 h
5.1: oxalyl chloride / benzene / 1 h / Heating
6.1: 0.451 g / AlCl3 / 4 h / 140 °C
With
aluminium trichloride; oxalyl dichloride; di-tert-butyl peroxide; hydrogen; magnesium; sodium iodide; HSiPh3;
In
diethyl ether; acetone; benzene;
2.1: Hunsdiecker reaction / 7.1: Friedel-Crafts reaction;
DOI:10.1021/jo060481q
