1,1'''-bis(p-iodobenzoyl)biferrocene

Base Information

Chemical Name:1,1'''-bis(p-iodobenzoyl)biferrocene
CAS No.:138208-52-3
Molecular Formula:C₃₄H₂₄Fe₂I₂O₂
Molecular Weight:830.066
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1'''-bis(p-iodobenzoyl)biferrocene

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Technology Process of 1,1'''-bis(p-iodobenzoyl)biferrocene

There total 1 articles about 1,1'''-bis(p-iodobenzoyl)biferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1,1''-biferrocene

: 1711-02-0
4-iodobenzoic acid chloride

: 138208-52-3
1,1'''-bis(p-iodobenzoyl)biferrocene

Guidance literature:: With AlCl₃; Na₂S₂O₃; In dichloromethane; under N2, Schlenk technique; mixt. of benzoyl chloride and excess AlCl3 (dried CH2Cl2, 0°C), filtration (glass wool, excess AlCl3), dropwise addn. to a soln. of biferrocene in dried CH2Cl2 (period of 1 h, 0°C), stirred (1-3 h, room temp.); poured into ice-water mixt., reduction with aq. Na2S2O3, sepn., organic layer washed with saturated aq. NaHCO3 and H2O, dried (MgSO4), evapn., chromy., recrystn. (benzene-hexane);
DOI:10.1021/om00038a012