Acetic acid (4aR,5S,6R,7S,8S,8aR)-8-acetoxy-6-hydroxy-2-phenyl-5-((3aR,4R,9aS,9bR)-2,2,8,8-tetramethyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-ylamino)-hexahydro-benzo[1,3]dioxin-7-yl ester

Base Information

• Chemical Name: Acetic acid (4aR,5S,6R,7S,8S,8aR)-8-acetoxy-6-hydroxy-2-phenyl-5-((3aR,4R,9aS,9bR)-2,2,8,8-tetramethyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-ylamino)-hexahydro-benzo[1,3]dioxin-7-yl ester
• CAS No.: 81692-21-9
• Molecular Formula: C₃₁H₄₁NO₁₁
• Molecular Weight: 603.667

Synonyms:

Chemical Property of Acetic acid (4aR,5S,6R,7S,8S,8aR)-8-acetoxy-6-hydroxy-2-phenyl-5-((3aR,4R,9aS,9bR)-2,2,8,8-tetramethyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-ylamino)-hexahydro-benzo[1,3]dioxin-7-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Useful:

Technology Process of Acetic acid (4aR,5S,6R,7S,8S,8aR)-8-acetoxy-6-hydroxy-2-phenyl-5-((3aR,4R,9aS,9bR)-2,2,8,8-tetramethyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-ylamino)-hexahydro-benzo[1,3]dioxin-7-yl ester

There total 19 articles about Acetic acid (4aR,5S,6R,7S,8S,8aR)-8-acetoxy-6-hydroxy-2-phenyl-5-((3aR,4R,9aS,9bR)-2,2,8,8-tetramethyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-ylamino)-hexahydro-benzo[1,3]dioxin-7-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

DL-4,7:5,6-di-O-isopropylidene-(1,4,6/5)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenylamine (81692-19-5,86900-54-1,90025-02-8,109718-74-3,109718-75-4,132016-22-9) + DL-3,4-di-O-acetyl-1,2-anhydro-5,7-O-benzylidene-(1,2,4,6/3,5)-6-hydroxymethyl-1,2,3,4,5-cyclohexanepentol (77144-73-1,101758-36-5) → N-<(1SR)-4,7:5,6-di-O-isopropylidene-4,5,6-trihydroxy-3-(hydroxymethyl)-2-cyclohexenyl>-(1RS)-3,4-di-O-acetyl-5,7-O-benzylidene-(1,3,5/2,4,6)-2,3,4,5-tetrahydroxy-6-(hydroxymethyl)cyclohexylamine (81692-21-9,81739-19-7,90761-65-2,90761-66-3,148347-69-7) + N-<(1SR)-4,7:5,6-di-O-isopropylidene-4,5,6-trihydroxy-3-(hydroxymethyl)-2-cyclohexenyl>-(1SR)-3,4-di-O-acetyl-5,7-O-benzylidene-(1,3,5/2,4,6)-2,3,4,5-tetrahydroxy-6-(hydroxymethyl)cyclohexylamine (81692-21-9,81739-19-7,90761-65-2,90761-66-3,148347-69-7) + DL-N-<(1SR)-4,7:5,6-di-O-isopropylidene-4,5,6-trihydroxy-3-(hydroxymethyl)-2-cyclohexenyl>-(1RS)-2,3-di-O-acetyl-4,7-O-benzylidene-(1,2,4/3,5,6)-2,3,4,6-tetrahydroxy-5-(hydroxymethyl)cyclohexylamine (81692-22-0,81739-20-0,90761-67-4,90761-68-5,148347-68-6)

Guidance literature:

In isopropyl alcohol; at 120 ℃; for 168h; Further byproducts given;

DOI:10.1021/jo00188a016

Reference yield: 18.0%

DL-4,7:5,6-di-O-isopropylidene-(1,4,6/5)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenylamine (81692-19-5,86900-54-1,90025-02-8,109718-74-3,109718-75-4,132016-22-9) + DL-3,4-di-O-acetyl-1,2-anhydro-5,7-O-benzylidene-(1,2,4,6/3,5)-6-hydroxymethyl-1,2,3,4,5-cyclohexanepentol (77144-73-1,101758-36-5) → N-<(1SR)-4,7:5,6-di-O-isopropylidene-4,5,6-trihydroxy-3-(hydroxymethyl)-2-cyclohexenyl>-(1RS)-3,4-di-O-acetyl-5,7-O-benzylidene-(1,3,5/2,4,6)-2,3,4,5-tetrahydroxy-6-(hydroxymethyl)cyclohexylamine (81692-21-9,81739-19-7,90761-65-2,90761-66-3,148347-69-7) + N-<(1SR)-4,7:5,6-di-O-isopropylidene-4,5,6-trihydroxy-3-(hydroxymethyl)-2-cyclohexenyl>-(1SR)-3,4-di-O-acetyl-5,7-O-benzylidene-(1,3,5/2,4,6)-2,3,4,5-tetrahydroxy-6-(hydroxymethyl)cyclohexylamine (81692-21-9,81739-19-7,90761-65-2,90761-66-3,148347-69-7) + DL-N-<(1SR)-4,7:5,6-di-O-isopropylidene-4,5,6-trihydroxy-3-(hydroxymethyl)-2-cyclohexenyl>-(1RS)-2,3-di-O-acetyl-4,7-O-benzylidene-(1,2,4/3,5,6)-2,3,4,6-tetrahydroxy-5-(hydroxymethyl)cyclohexylamine (81692-22-0,81739-20-0,90761-67-4,90761-68-5,148347-68-6)

Guidance literature:

In isopropyl alcohol; at 120 ℃; for 168h; Further byproducts given;

DOI:10.1021/jo00188a016

Reference yield: 18.0%

DL-4,7:5,6-di-O-isopropylidene-(1,4,6/5)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenylamine (81692-19-5,86900-54-1,90025-02-8,109718-74-3,109718-75-4,132016-22-9) + DL-3,4-di-O-acetyl-1,2-anhydro-5,7-O-benzylidene-(1,2,4,6/3,5)-6-hydroxymethyl-1,2,3,4,5-cyclohexanepentol (77144-73-1,101758-36-5) → N-<(1SR)-4,7:5,6-di-O-isopropylidene-4,5,6-trihydroxy-3-(hydroxymethyl)-2-cyclohexenyl>-(1SR)-3,4-di-O-acetyl-5,7-O-benzylidene-(1,3,5/2,4,6)-2,3,4,5-tetrahydroxy-6-(hydroxymethyl)cyclohexylamine (81692-21-9,81739-19-7,90761-65-2,90761-66-3,148347-69-7) + DL-N-<(1SR)-4,7:5,6-di-O-isopropylidene-4,5,6-trihydroxy-3-(hydroxymethyl)-2-cyclohexenyl>-(1SR)-2,3-di-O-acetyl-4,7-O-benzylidene-(1,2,4/3,5,6)-2,3,4,6-tetrahydroxy-5-(hydroxymethyl)cyclohexylamine (81692-22-0,81739-20-0,90761-67-4,90761-68-5,148347-68-6) + DL-N-<(1SR)-4,7:5,6-di-O-isopropylidene-4,5,6-trihydroxy-3-(hydroxymethyl)-2-cyclohexenyl>-(1RS)-2,3-di-O-acetyl-4,7-O-benzylidene-(1,2,4/3,5,6)-2,3,4,6-tetrahydroxy-5-(hydroxymethyl)cyclohexylamine (81692-22-0,81739-20-0,90761-67-4,90761-68-5,148347-68-6)

Guidance literature:

In isopropyl alcohol; at 120 ℃; for 168h; Further byproducts given;

DOI:10.1021/jo00188a016

upstream raw materials:

DL-4,7:5,6-di-O-isopropylidene-(1,4,6/5)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenylamine

DL-3,4-di-O-acetyl-1,2-anhydro-5,7-O-benzylidene-(1,2,4,6/3,5)-6-hydroxymethyl-1,2,3,4,5-cyclohexanepentol

DL-(1,3/2)-1,2,3-tri-O-acetyl-4-methylene-5-cyclohexene-1,2,3-triol

DL-Tetra-O-acetyl-(1,3,6/2)-6-azido-4-(hydroxymethyl)-4-cyclohexene-1,2,3-triol

Downstream raw materials:

N-<(1SR)-(1,4,6/5)-4,5,6-trihydroxy-3-(hydroxymethyl)-2-cyclohexenyl>-(1SR)-(1,3,5/2,4,6)-2,3,4,5-tetrahydroxy-6-(hydroxymethyl)cyclohexylamine nonaacetate

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