1,3-di-mesityl-1,3,2-diazaphospholenium tricarbonyl cobaltate

Base Information

• Chemical Name: 1,3-di-mesityl-1,3,2-diazaphospholenium tricarbonyl cobaltate
• CAS No.: 869217-56-1
• Molecular Formula: C₂₃H₂₄CoN₂O₃P
• Molecular Weight: 466.422
• Mol file: 869217-56-1.mol

Synonyms:

Chemical Property of 1,3-di-mesityl-1,3,2-diazaphospholenium tricarbonyl cobaltate

Chemical Property:

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Technology Process of 1,3-di-mesityl-1,3,2-diazaphospholenium tricarbonyl cobaltate

There total 1 articles about 1,3-di-mesityl-1,3,2-diazaphospholenium tricarbonyl cobaltate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

thallium(I) tetracarbonylcobaltate (38991-21-8) + 2-chloro-1,3-bis(2,4,6-trimethylphenyl)-1,3,2-diazaphosphalene (306283-67-0) → 1,3-di-mesityl-1,3,2-diazaphospholenium tricarbonyl cobaltate (869217-56-1)

Guidance literature:

In toluene; byproducts: TlCl, CO; 2 h stirring at room temp., (Ar); filtration, vac. evapn., recrystn. (CH3CN, -25 °C), elem. anal.;

DOI:10.1002/zaac.200400538

upstream raw materials:

thallium(I) tetracarbonylcobaltate

2-chloro-1,3-bis(2,4,6-trimethylphenyl)-1,3,2-diazaphosphalene