(Me₃Sn)2CHCH₂PPh₂

Base Information

Chemical Name:(Me₃Sn)2CHCH₂PPh₂
CAS No.:120726-18-3
Molecular Formula:C₂₀H₃₁PSn₂
Molecular Weight:539.86
Hs Code.:

(Me<sub>3</sub>Sn)2CHCH<sub>2</sub>PPh<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Me₃Sn)2CHCH₂PPh₂

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Technology Process of (Me₃Sn)2CHCH₂PPh₂

There total 4 articles about (Me₃Sn)2CHCH₂PPh₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1631-73-8
trimethylstannane

: 6104-47-8
ethynyldiphenylphosphine

: 120726-18-3
(Me₃Sn)2CHCH₂PPh₂

Guidance literature:: Irradiation (UV/VIS); Two equiv. of Me3SnH with ethynyldiphenylphosphine are irradiated under Ar for 20 h.; an oil is obtained after distn., elem. anal.;
DOI:10.1016/0022-328X(89)85311-2

Reference yield: 69.0%

: 21037-93-4
Me₃SnC₂PPh₂

: 1631-73-8
trimethylstannane

: 120726-18-3
(Me₃Sn)2CHCH₂PPh₂

: 120726-26-3
(Me₃Sn)2CCH(PPh₂)

Guidance literature:: Irradiation (UV/VIS); An equimolar mixture of Me3SnH and the alkynylphosphine are irradiated in a quartz Schlenk tube for 12 h under Ar.; purifn. by distn., elem. anal.;
DOI:10.1016/0022-328X(89)85311-2

Reference yield: 11.0%

: 1631-73-8
trimethylstannane

: 6104-47-8
ethynyldiphenylphosphine

: 120726-18-3
(Me₃Sn)2CHCH₂PPh₂

: 125708-50-1
(Z)-(trimethylstannyl)CHCH(diphenylphosphine)

: 125708-50-1
(E)-(trimethylstannyl)CHCH(diphenylphosphine)

Guidance literature:: Irradiation (UV/VIS); An equimolar mixture of Me3SnH and the alkynylphosphine are irradiated in a quartz Schlenk tube for 12 h under Ar.; purifn. by distn., elem. anal., yields 73 % (Z/E 1/5);
DOI:10.1016/0022-328X(89)85311-2