{(C₄H₉Sn(OH)O₂P(OC₆H₅)2)3O}⁽¹⁺⁾*{O₂P(OC₆H₅)2}^(1-)={(C₄H₉Sn(OH)O₂P(OC₆H₅)2)3O}{O₂P(OC₆H₅)2}

Base Information

• Chemical Name: {(C₄H₉Sn(OH)O₂P(OC₆H₅)2)3O}⁽¹⁺⁾*{O₂P(OC₆H₅)2}^(1-)={(C₄H₉Sn(OH)O₂P(OC₆H₅)2)3O}{O₂P(OC₆H₅)2}
• CAS No.: 115270-33-2
• Molecular Formula: C₁₂H₁₀O₄P*C₄₈H₆₀O₁₆P₃Sn₃
• Molecular Weight: 1591.23
• Mol file: 115270-33-2.mol

Synonyms:

Chemical Property of {(C₄H₉Sn(OH)O₂P(OC₆H₅)2)3O}⁽¹⁺⁾*{O₂P(OC₆H₅)2}^(1-)={(C₄H₉Sn(OH)O₂P(OC₆H₅)2)3O}{O₂P(OC₆H₅)2}

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of {(C₄H₉Sn(OH)O₂P(OC₆H₅)2)3O}⁽¹⁺⁾*{O₂P(OC₆H₅)2}^(1-)={(C₄H₉Sn(OH)O₂P(OC₆H₅)2)3O}{O₂P(OC₆H₅)2}

There total 1 articles about {(C₄H₉Sn(OH)O₂P(OC₆H₅)2)3O}⁽¹⁺⁾*{O₂P(OC₆H₅)2}^(1-)={(C₄H₉Sn(OH)O₂P(OC₆H₅)2)3O}{O₂P(OC₆H₅)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

diphenyl hydrogen phosphate (838-85-7) + n-butylstannoic acid (2273-43-0) → {(C4H9Sn(OH)O2P(OC6H5)2)3O}(1+)*{O2P(OC6H5)2}(1-)={(C4H9Sn(OH)O2P(OC6H5)2)3O}{O2P(OC6H5)2} (115270-33-2)

Guidance literature:

In benzene; soln. of diphenyl phosphate and n-butylstannoic acid in benzene (standing at 25°C, 48 h), removal of solvent (<20°C), addn. of diethyl ether, standing (25°C, 48 h), filtration from insol. material; removal of solvent (20°C); no successful purifn. from traces of water and other impurities, purity about 96 %;

Reference yield: 65.0%

{(C4H9Sn(OH)O2P(OC6H5)2)3O}(1+)*{O2P(OC6H5)2}(1-)={(C4H9Sn(OH)O2P(OC6H5)2)3O}{O2P(OC6H5)2} (115270-33-2) → hexameric n-butyloxotin diphenyl phosphate (115270-27-4)

Guidance literature:

In toluene; benzene; byproducts: water; heating in benzene (reflux, 1/2 h; azeotropic removal of water), further heating in toluene (azeotropic removal of water), concn. of the residue;

upstream raw materials:

diphenyl hydrogen phosphate

n-butylstannoic acid

Downstream raw materials:

hexameric n-butyloxotin diphenyl phosphate

Refernces