copper(II) meso-tetraphenyl-1-(3-propionic acid)porphyrin

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Chemical Name:copper(II) meso-tetraphenyl-1-(3-propionic acid)porphyrin
CAS No.:83037-22-3
Molecular Formula:C₄₇H₃₂CuN₄O₂
Molecular Weight:748.343
Hs Code.:

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Chemical Property of copper(II) meso-tetraphenyl-1-(3-propionic acid)porphyrin

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Technology Process of copper(II) meso-tetraphenyl-1-(3-propionic acid)porphyrin

There total 1 articles about copper(II) meso-tetraphenyl-1-(3-propionic acid)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 83037-21-2
copper(II) meso-tetraphenyl-1-(2-ethoxycarbonylethyl)porphyrin

: 83037-22-3
copper(II) meso-tetraphenyl-1-(3-propionic acid)porphyrin

Guidance literature:: With potassium hydroxide; In pyridine; methanol; KOH in methanol was added to the soln. of the Cu-compd. in pyridine, then the soln. was stirred for 24 h at room temp.; the solvent was removed and the residue was neutralized with aq. HCl, the product was extd. into CHCl3 and the soln. was dried over Na2SO4, chromd. on silica gel and recrystd. from CHCl3/heptane;
DOI:10.1139/v82-204

Reference yield: 67.0%

: 83037-22-3
copper(II) meso-tetraphenyl-1-(3-propionic acid)porphyrin

: 34272-83-8
2,2,5,5-tetramethyl-3-aminopyrrolidine-1-oxyl

: 83037-27-8
copper(II) meso-tetraphenyl-1-<3-(N-(2,2,5,5-tetramethylpyrrolidinyl-1-oxy))propionamido>porphyrin

Guidance literature:: With oxalyl dichloride; In tetrahydrofuran; pyridine; benzene; the Cu-compd. in benzene was stirred with oxalyl chloride at room temp. for 2 h, then the solvent was removed in vac., the residue was kept in vac. for 2 h, then dissolved in THF and pyridine, then the pyrrolidinyl compd. was added and refluxed for 6 h; the solvent was removed in vac., the residue was chromd. on silica gel and recrystd. from CHCl3/heptane; elem. anal.;
DOI:10.1139/v82-204

Reference yield: 61.0%

: 83037-22-3
copper(II) meso-tetraphenyl-1-(3-propionic acid)porphyrin

: 14691-88-4,78774-22-8
4-amino-2,2,6,6-tetramethyl-1-piperidine-1-oxyl

: 83037-25-6
copper(II) meso-tetraphenyl-1-<3-(N-(2,2,6,6-tetramethylpiperidinyl-1-oxy))propionamido>porphyrin

Guidance literature:: With oxalyl dichloride; In tetrahydrofuran; pyridine; benzene; the Cu-compd. in benzene was stirred with oxalyl chloride at room temp. for 2 h, then the solvent was removed in vac., the residue was kept in vac. for 2 h, then dissolved in THF and pyridine, then the piperidinyl compd. was added and refluxed for 6 h; the solvent was removed in vac., the residue was chromd. on silica gel and recrystd. from CHCl3/heptane; elem. anal.;
DOI:10.1139/v82-204