di(isopropyl)carbamic acid (S)-1-(4,4,5,5-tetramethyl[1,3,2]-dioxaborolan-2-yl)-3-(3,4,5-trimethoxyphenyl)propyl ester

Base Information

Chemical Name:di(isopropyl)carbamic acid (S)-1-(4,4,5,5-tetramethyl[1,3,2]-dioxaborolan-2-yl)-3-(3,4,5-trimethoxyphenyl)propyl ester
CAS No.:902141-73-5
Molecular Formula:C₂₅H₄₂BNO₇
Molecular Weight:479.422
Hs Code.:

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Chemical Property of di(isopropyl)carbamic acid (S)-1-(4,4,5,5-tetramethyl[1,3,2]-dioxaborolan-2-yl)-3-(3,4,5-trimethoxyphenyl)propyl ester

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Technology Process of di(isopropyl)carbamic acid (S)-1-(4,4,5,5-tetramethyl[1,3,2]-dioxaborolan-2-yl)-3-(3,4,5-trimethoxyphenyl)propyl ester

There total 1 articles about di(isopropyl)carbamic acid (S)-1-(4,4,5,5-tetramethyl[1,3,2]-dioxaborolan-2-yl)-3-(3,4,5-trimethoxyphenyl)propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 902119-99-7
di(isopropyl)carbamic acid 3-(3,4,5-trimethoxyphenyl)propyl ester

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 902480-73-3,902141-73-5
di(isopropyl)carbamic acid (S)-1-(4,4,5,5-tetramethyl[1,3,2]-dioxaborolan-2-yl)-3-(3,4,5-trimethoxyphenyl)propyl ester

Guidance literature:: With s-BuLi; (-)-sparteine; In diethyl ether; addn. of soln. of s-BuLi to soln. of carbamate and sparteine in anhydrous ether at -78°C, stirring for 5 h, addn. of ether and then boroncompd., stirring for 1 h at -78°C; addn. of water, warming to room temp., extn. (ether), drying under Na2SO4, filtration, concn., chromy. (silica gel, CH2Cl2-ether);
DOI:10.1039/b603857c