(2S,2'S)-2,2'-bis-benzoylamino-3,3'-(5,5'-dimethoxy-3-oxo-3,4-dihydro-[2,2']bi[benzo[1,4]thiazinylidene]-7,7'-diyl)-bis-propionic acid dimethyl ester

Base Information

Chemical Name:(2S,2'S)-2,2'-bis-benzoylamino-3,3'-(5,5'-dimethoxy-3-oxo-3,4-dihydro-[2,2']bi[benzo[1,4]thiazinylidene]-7,7'-diyl)-bis-propionic acid dimethyl ester
CAS No.:23416-86-6
Molecular Formula:C₄₀H₃₆N₄O₉S₂
Molecular Weight:780.879
Hs Code.:

(2<i>S</i>,2'<i>S</i>)-2,2'-bis-benzoylamino-3,3'-(5,5'-dimethoxy-3-oxo-3,4-dihydro-[2,2']bi[benzo[1,4]thiazinylidene]-7,7'-diyl)-bis-propionic acid dimethyl ester

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Chemical Property of (2S,2'S)-2,2'-bis-benzoylamino-3,3'-(5,5'-dimethoxy-3-oxo-3,4-dihydro-[2,2']bi[benzo[1,4]thiazinylidene]-7,7'-diyl)-bis-propionic acid dimethyl ester

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Technology Process of (2S,2'S)-2,2'-bis-benzoylamino-3,3'-(5,5'-dimethoxy-3-oxo-3,4-dihydro-[2,2']bi[benzo[1,4]thiazinylidene]-7,7'-diyl)-bis-propionic acid dimethyl ester

There total 4 articles about (2S,2'S)-2,2'-bis-benzoylamino-3,3'-(5,5'-dimethoxy-3-oxo-3,4-dihydro-[2,2']bi[benzo[1,4]thiazinylidene]-7,7'-diyl)-bis-propionic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25565-25-7
5-Cystein-S-yldopa

: 23416-86-6
(2S,2'S)-2,2'-bis-benzoylamino-3,3'-(5,5'-dimethoxy-3-oxo-3,4-dihydro-[2,2']bi[benzo[1,4]thiazinylidene]-7,7'-diyl)-bis-propionic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1) O₂, alcaline, 2) acid

2: aq. NaOH, NaHCO₃ / diethyl ether / 2 h / 4 °C

3: methanol; CHCl₃; diethyl ether / 0.5 h

With sodium hydroxide; oxygen; sodium hydrogencarbonate; In methanol; diethyl ether; chloroform;

Reference yield:

: 23416-50-4
2,2'-diamino-3,3'-(5,5'-dihydroxy-3-oxo-3,4-dihydro-[2,2']bi[benzo[1,4]thiazinylidene]-7,7'-diyl)-bis-propionic acid

: 23416-86-6
(2S,2'S)-2,2'-bis-benzoylamino-3,3'-(5,5'-dimethoxy-3-oxo-3,4-dihydro-[2,2']bi[benzo[1,4]thiazinylidene]-7,7'-diyl)-bis-propionic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH, NaHCO₃ / diethyl ether / 2 h / 4 °C

2: methanol; CHCl₃; diethyl ether / 0.5 h

With sodium hydroxide; sodium hydrogencarbonate; In methanol; diethyl ether; chloroform;

Reference yield:

: 23416-49-1,32214-49-6
7,7'-bis-(2-amino-2-carboxy-ethyl)-5,5'-dihydroxy-3'-oxo-3',4'-dihydro-[2,2']bi[benzo[1,4]thiazinylidene]-3-carboxylic acid

: 23416-86-6
(2S,2'S)-2,2'-bis-benzoylamino-3,3'-(5,5'-dimethoxy-3-oxo-3,4-dihydro-[2,2']bi[benzo[1,4]thiazinylidene]-7,7'-diyl)-bis-propionic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: acid / Heating

2: aq. NaOH, NaHCO₃ / diethyl ether / 2 h / 4 °C

3: methanol; CHCl₃; diethyl ether / 0.5 h

With sodium hydroxide; sodium hydrogencarbonate; In methanol; diethyl ether; chloroform;