[Pd(C₁₁H₈N)((C₆H₅)3PC(O₂CCH₃)CSNHC₆H₅)(C₆H₅)3P]⁽¹⁺⁾*ClO₄^(1-)=[Pd(C₁₁H₈N)((C₆H₅)3PC(O₂CCH₃)CSNHC₆H₅)(C₆H₅)3P][ClO₄]

Base Information

• Chemical Name: [Pd(C₁₁H₈N)((C₆H₅)3PC(O₂CCH₃)CSNHC₆H₅)(C₆H₅)3P]⁽¹⁺⁾*ClO₄^(1-)=[Pd(C₁₁H₈N)((C₆H₅)3PC(O₂CCH₃)CSNHC₆H₅)(C₆H₅)3P][ClO₄]
• CAS No.: 952303-08-1
• Molecular Formula: C₅₇H₄₇N₂O₂P₂PdS*ClO₄
• Molecular Weight: 1091.9
• Mol file: 952303-08-1.mol

Synonyms:

Chemical Property of [Pd(C₁₁H₈N)((C₆H₅)3PC(O₂CCH₃)CSNHC₆H₅)(C₆H₅)3P]⁽¹⁺⁾*ClO₄^(1-)=[Pd(C₁₁H₈N)((C₆H₅)3PC(O₂CCH₃)CSNHC₆H₅)(C₆H₅)3P][ClO₄]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Pd(C₁₁H₈N)((C₆H₅)3PC(O₂CCH₃)CSNHC₆H₅)(C₆H₅)3P]⁽¹⁺⁾*ClO₄^(1-)=[Pd(C₁₁H₈N)((C₆H₅)3PC(O₂CCH₃)CSNHC₆H₅)(C₆H₅)3P][ClO₄]

There total 2 articles about [Pd(C₁₁H₈N)((C₆H₅)3PC(O₂CCH₃)CSNHC₆H₅)(C₆H₅)3P]⁽¹⁺⁾*ClO₄^(1-)=[Pd(C₁₁H₈N)((C₆H₅)3PC(O₂CCH₃)CSNHC₆H₅)(C₆H₅)3P][ClO₄] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

[Pd(C11H8N)((C6H5)3PC(O2CCH3)CSNHC6H5)](1+)*ClO4(1-)=[Pd(C11H8N)((C6H5)3PC(O2CCH3)CSNHC6H5)][ClO4] (952303-04-7) + triphenylphosphine (603-35-0) → [Pd(C11H8N)((C6H5)3PC(O2CCH3)CSNHC6H5)(C6H5)3P](1+)*ClO4(1-)=[Pd(C11H8N)((C6H5)3PC(O2CCH3)CSNHC6H5)(C6H5)3P][ClO4] (952303-08-1)

Guidance literature:

In dichloromethane-d2; 1:1 mixt.; NMR;

DOI:10.1002/ejic.200600599

Reference yield:

di-μ-chlorobis{(2-phenylpyridine)palladium(II)} + Phenylthiocarbamoyl-(triphenyl-λ5-phosphanylidene)-acetic acid methyl ester (952303-35-4) → [Pd(C11H8N)((C6H5)3PC(O2CCH3)CSNHC6H5)(C6H5)3P](1+)*ClO4(1-)=[Pd(C11H8N)((C6H5)3PC(O2CCH3)CSNHC6H5)(C6H5)3P][ClO4] (952303-08-1)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran

2: dichloromethane-d2

In tetrahydrofuran; dichloromethane-d2;

DOI:10.1002/ejic.200600599

upstream raw materials:

[Pd(C₁₁H₈N)((C₆H₅)3PC(O₂CCH₃)CSNHC₆H₅)]⁽¹⁺⁾*ClO₄^(1-)=[Pd(C₁₁H₈N)((C₆H₅)3PC(O₂CCH₃)CSNHC₆H₅)][ClO₄]

triphenylphosphine

Phenylthiocarbamoyl-(triphenyl-λ⁵-phosphanylidene)-acetic acid methyl ester