Technology Process of C24H23BrO6
There total 4 articles about C24H23BrO6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dmap; triethylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere
2.1: N,N-dimethyl-aniline / dichloromethane / 0.25 h / Inert atmosphere; Cooling with ice
2.2: 0.5 h / 0 - 20 °C / Inert atmosphere
3.1: bis(N-tert-butylsalicylaldiminato)copper(II) / toluene / 1 h / Inert atmosphere; Reflux
4.1: acetic acid / tetrahydrofuran; water
With
dmap; bis(N-tert-butylsalicylaldiminato)copper(II); acetic acid; N,N-dimethyl-aniline; triethylamine;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo102033h
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N,N-dimethyl-aniline / dichloromethane / 0.25 h / Inert atmosphere; Cooling with ice
1.2: 0.5 h / 0 - 20 °C / Inert atmosphere
2.1: bis(N-tert-butylsalicylaldiminato)copper(II) / toluene / 1 h / Inert atmosphere; Reflux
3.1: acetic acid / tetrahydrofuran; water
With
bis(N-tert-butylsalicylaldiminato)copper(II); acetic acid; N,N-dimethyl-aniline;
In
tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1021/jo102033h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: bis(N-tert-butylsalicylaldiminato)copper(II) / toluene / 1 h / Inert atmosphere; Reflux
2: acetic acid / tetrahydrofuran; water
With
bis(N-tert-butylsalicylaldiminato)copper(II); acetic acid;
In
tetrahydrofuran; water; toluene;
DOI:10.1021/jo102033h