C₁₂H₁₀⁽²⁾HNOS

Base Information

• Chemical Name: C₁₂H₁₀⁽²⁾HNOS
• CAS No.: 1345470-53-2
• Molecular Formula: C₁₂H₁₁NOS
• Molecular Weight: 218.284

Synonyms:

Chemical Property of C₁₂H₁₀⁽²⁾HNOS

Chemical Property:

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Technology Process of C₁₂H₁₀⁽²⁾HNOS

There total 1 articles about C₁₂H₁₀⁽²⁾HNOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-bromophenylsulfanyl)pyridine (1210812-23-9) → C12H10(2)HNOS (1345470-53-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid

3.1: silver(I) acetate; palladium diacetate; p-benzoquinone / tert-Amyl alcohol / 2 h / 100 °C / Under atmospheric air

With n-butyllithium; silver(I) acetate; palladium diacetate; 3-chloro-benzenecarboperoxoic acid; p-benzoquinone; In tetrahydrofuran; tert-Amyl alcohol; hexane;

DOI:10.1021/jo2018137

upstream raw materials:

2-(2-bromophenylsulfanyl)pyridine

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