C₃₅H₃₈O₁₂

Base Information

Chemical Name:C₃₅H₃₈O₁₂
CAS No.:1326704-17-9
Molecular Formula:C₃₅H₃₈O₁₂
Molecular Weight:650.68
Hs Code.:

C<sub>35</sub>H<sub>38</sub>O<sub>12</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₅H₃₈O₁₂

Chemical Property:

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Technology Process of C₃₅H₃₈O₁₂

There total 9 articles about C₃₅H₃₈O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1326704-16-8
(2S)-6-iodo-1-[(4-methoxybenzyl)oxy]hex-5-yn-2-yl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: hepta-1,3,5-triyn-1-yl(trimethyl)silane

: 1326704-17-9
C₃₅H₃₈O₁₂

Guidance literature:: (2S)-6-iodo-1-[(4-methoxybenzyl)oxy]hex-5-yn-2-yl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside; hepta-1,3,5-triyn-1-yl(trimethyl)silane; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; silver fluoride; potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h; Inert atmosphere;

With methanol; In N,N-dimethyl-formamide; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/chem.201100986

Reference yield:

: (2S)-6-(trimethylsilyl)hex-5-yne-1,2-diol

: 1326704-17-9
C₃₅H₃₈O₁₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: di(n-butyl)tin oxide / toluene / 2 h / Reflux

1.2: 20 °C

1.3: 5 h / Reflux

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

3.1: dichloromethane / 0.17 h / 20 °C / Molecular sieve

3.2: 16 h / -60 °C

4.1: N-iodo-succinimide; silver nitrate / acetone / 2 h / 20 °C / Darkness

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; silver fluoride; potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere

5.2: 16 h / 20 °C / Inert atmosphere

With N-iodo-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; silver fluoride; di(n-butyl)tin oxide; potassium carbonate; silver nitrate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1002/chem.201100986

Reference yield:

: 37176-72-0
6-trimethylsianyl-hexa-3,5-diyn-2-one

: 1326704-17-9
C₃₅H₃₈O₁₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine / dichloromethane / 0.25 h / 0 °C

1.2: 16 h / 45 °C

2.1: n-butyllithium / hexane / -78 - -40 °C / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; silver fluoride; potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere

3.2: 16 h / 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; silver fluoride; potassium carbonate; triphenylphosphine; In hexane; dichloromethane; N,N-dimethyl-formamide; 1.1: Corey-Fuchs reaction / 1.2: Corey-Fuchs reaction / 2.1: Corey-Fuchs reaction;
DOI:10.1002/chem.201100986