Technology Process of C15H16F3NO3S
There total 4 articles about C15H16F3NO3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Ag(1+)*C48H28O4P(1-);
In
tetrachloromethane;
at 25 ℃;
for 24h;
optical yield given as %ee;
enantioselective reaction;
Molecular sieve;
Darkness;
DOI:10.1002/asia.201101029
- Guidance literature:
-
Multi-step reaction with 4 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
2: hydrazine hydrate / ethanol / 3 h / Reflux
3: triethylamine / dichloromethane / 0.67 h / 0 °C / Inert atmosphere
4: Ag(1+)*C48H28O4P(1-) / tetrachloromethane / 24 h / 25 °C / Molecular sieve; Darkness
With
di-isopropyl azodicarboxylate; Ag(1+)*C48H28O4P(1-); hydrazine hydrate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; tetrachloromethane; ethanol; dichloromethane;
1: Mitsunobu reaction;
DOI:10.1002/asia.201101029
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrazine hydrate / ethanol / 3 h / Reflux
2: triethylamine / dichloromethane / 0.67 h / 0 °C / Inert atmosphere
3: Ag(1+)*C48H28O4P(1-) / tetrachloromethane / 24 h / 25 °C / Molecular sieve; Darkness
With
Ag(1+)*C48H28O4P(1-); hydrazine hydrate; triethylamine;
In
tetrachloromethane; ethanol; dichloromethane;
DOI:10.1002/asia.201101029
