C₁₀H₁₅FO₅

Base Information

Chemical Name:C₁₀H₁₅FO₅
CAS No.:1336914-68-1
Molecular Formula:C₁₀H₁₅FO₅
Molecular Weight:234.225
Hs Code.:

C<sub>10</sub>H<sub>15</sub>FO<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₀H₁₅FO₅

Chemical Property:

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Technology Process of C₁₀H₁₅FO₅

There total 25 articles about C₁₀H₁₅FO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₁₆O₆

: C₁₀H₁₅FO₅

: 1336914-68-1
C₁₀H₁₅FO₅

Guidance literature:: With diethylamino-sulfur trifluoride; In tetrahydrofuran; at -40 ℃; for 0.333333h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol202315m

Reference yield:

: 865484-73-7
tert-butyl ((2S,6S)-6-methyl-5-oxo-5,6-dihydro-2H-pyran-2-yl) carbonate

: C₁₀H₁₅FO₅

: 1336914-68-1
C₁₀H₁₅FO₅

Guidance literature:: Multi-step reaction with 12 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine / dichloromethane / 4 h / Inert atmosphere; Cooling with ice

2: L-Selectride / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

3: tetrahydrofuran / 4.08 h / -78 - -25 °C / Inert atmosphere

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium chloride / tetrahydrofuran / 23 - 80 °C / Inert atmosphere

5: hydrogenchloride; water; sodium hydroxide / Inert atmosphere

6: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone; tert-butyl alcohol / 72 h / 0 - 23 °C / Inert atmosphere

7: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

8: sodium periodate; ruthenium trichloride / tetrachloromethane; water; acetonitrile / 1 h / Inert atmosphere; Cooling with ice

9: N,N-dimethyl-formamide / 4.25 h / 23 - 50 °C / Inert atmosphere

10: sulfuric acid; water / tetrahydrofuran / 1 h / 23 °C / Inert atmosphere

11: palladium 10% on activated carbon; hydrogen / water; ethyl acetate / 16.5 h / 23 °C / 760.05 Torr

12: diethylamino-sulfur trifluoride / tetrahydrofuran / 0.33 h / -40 °C / Inert atmosphere

With hydrogenchloride; ruthenium trichloride; sodium periodate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; diethylamino-sulfur trifluoride; sulfuric acid; palladium 10% on activated carbon; water; hydrogen; L-Selectride; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; lithium chloride; sodium hydroxide; In tetrahydrofuran; tetrachloromethane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ol202315m

Reference yield:

: 1192-62-7,80145-44-4
1-(2-furyl)-1-ethanone

: C₁₀H₁₅FO₅

: 1336914-68-1
C₁₀H₁₅FO₅

Guidance literature:: Multi-step reaction with 13 steps

1.1: trans-RuCl₂-[(R)-xylbinap][(R)-daipen]; hydrogen / 37503.8 Torr

2.1: bromine / methanol; diethyl ether / 1.08 h / -78 - -30 °C / Inert atmosphere

2.2: 0.08 h / 23 °C / Inert atmosphere

3.1: L-Selectride / tetrahydrofuran / 1.25 h / -78 °C / Inert atmosphere

4.1: tetrahydrofuran / 7.08 h / -78 - -25 °C / Inert atmosphere

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium chloride / tetrahydrofuran / 23 - 80 °C / Inert atmosphere

6.1: water / tetrahydrofuran; water; pentane / Inert atmosphere

7.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone; tert-butyl alcohol / 73 h / 0 - 23 °C / Inert atmosphere; Cooling with ice

8.1: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

9.1: sodium periodate; ruthenium trichloride / tetrachloromethane; water; acetonitrile / 1 h / Inert atmosphere; Cooling with ice

10.1: N,N-dimethyl-formamide / 23 - 50 °C / Inert atmosphere

11.1: sulfuric acid; water / tetrahydrofuran / 1 h / 23 °C / Inert atmosphere

12.1: acetic acid / water / 2 h / 95 °C / Inert atmosphere

13.1: diethylamino-sulfur trifluoride / tetrahydrofuran / 0.33 h / -40 °C / Inert atmosphere

With ruthenium trichloride; sodium periodate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; diethylamino-sulfur trifluoride; sulfuric acid; trans-RuCl₂-[(R)-xylbinap][(R)-daipen]; water; hydrogen; bromine; L-Selectride; acetic acid; 4-methylmorpholine N-oxide; triethylamine; lithium chloride; In tetrahydrofuran; methanol; tetrachloromethane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; tert-butyl alcohol; pentane;
DOI:10.1021/ol202315m