Technology Process of C17H18Cl2FN3O
There total 7 articles about C17H18Cl2FN3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triisopropylsilyl trifluoromethanesulfonate; trifluoroacetic acid;
In
water;
at 20 ℃;
DOI:10.1021/jm300303e
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-ethyl-N,N-diisopropylamine / methanol; dichloromethane / 20 °C
2.1: potassium carbonate / water; acetonitrile / 20 °C
3.1: hydrazine / tetrahydrofuran / 0.5 h / 65 °C / Microwave irradiation
4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 0 - 20 °C
4.2: 20 °C
5.1: triisopropylsilyl trifluoromethanesulfonate; trifluoroacetic acid / water / 20 °C
With
triisopropylsilyl trifluoromethanesulfonate; potassium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; hydrazine;
In
tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/jm300303e
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrazine / tetrahydrofuran / 0.5 h / 65 °C / Microwave irradiation
2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 0 - 20 °C
2.2: 20 °C
3.1: triisopropylsilyl trifluoromethanesulfonate; trifluoroacetic acid / water / 20 °C
With
triisopropylsilyl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; hydrazine;
In
tetrahydrofuran; water;
DOI:10.1021/jm300303e
