C₃₃H₂₉F₁₀N₅

Base Information

Chemical Name:C₃₃H₂₉F₁₀N₅
CAS No.:1283098-40-7
Molecular Formula:C₃₃H₂₉F₁₀N₅
Molecular Weight:685.611
Hs Code.:

C<sub>33</sub>H<sub>29</sub>F<sub>10</sub>N<sub>5</sub>

Synonyms:

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Chemical Property of C₃₃H₂₉F₁₀N₅

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Technology Process of C₃₃H₂₉F₁₀N₅

There total 7 articles about C₃₃H₂₉F₁₀N₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1283098-39-4
C₄₁H₃₅F₁₀N₅O₂

: 1283098-40-7
C₃₃H₂₉F₁₀N₅

Guidance literature:: With cyclohexa-1,4-diene; palladium 10% on activated carbon; In methanol; at 50 ℃; for 14h; Inert atmosphere;
DOI:10.1021/ja110842s

Reference yield:

: 327022-92-4
1-pentafluorophenyl-3-buten-1-ol

: 1283098-40-7
C₃₃H₂₉F₁₀N₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: acetic acid / methanol / 12 h / 50 °C / Inert atmosphere

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 12 h / 50 °C / Inert atmosphere

5.1: palladium 10% on activated carbon; cyclohexa-1,4-diene / methanol / 14 h / 50 °C / Inert atmosphere

With oxalyl dichloride; cyclohexa-1,4-diene; dimethylsulfide borane complex; palladium 10% on activated carbon; acetic acid; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja110842s

Reference yield:

: 1283098-36-1
1-(perfluorophenyl)butane-1,4-diol

: 1283098-40-7
C₃₃H₂₉F₁₀N₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: acetic acid / methanol / 12 h / 50 °C / Inert atmosphere

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 12 h / 50 °C / Inert atmosphere

4.1: palladium 10% on activated carbon; cyclohexa-1,4-diene / methanol / 14 h / 50 °C / Inert atmosphere

With oxalyl dichloride; cyclohexa-1,4-diene; palladium 10% on activated carbon; acetic acid; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja110842s