C₄₈H₄₅N₉O₆

Base Information

• Chemical Name: C₄₈H₄₅N₉O₆
• CAS No.: 1312807-30-9
• Molecular Formula: C₄₈H₄₅N₉O₆
• Molecular Weight: 843.942
• Mol file: 1312807-30-9.mol

Synonyms:

Chemical Property of C₄₈H₄₅N₉O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₈H₄₅N₉O₆

There total 4 articles about C₄₈H₄₅N₉O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

C27H30N6O3 + phenyl isocyanate (103-71-9) → C48H45N9O6 (1312807-30-9)

Guidance literature:

In chloroform; for 5h; Reflux;

DOI:10.1080/10610278.2010.514909

Reference yield:

3-amino-5-nitro-benzoic acid (618-84-8) → C48H45N9O6 (1312807-30-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: sulfuric acid / ethanol / 6 h / 80 °C

1.2: 6 h / 80 °C

1.3: 6 h / 90 °C

2.1: dichlorotriphenyl-λ⁴-phosphane / 1,1,2,2-tetrachloroethane / 6 h / 120 °C

3.1: palladium on activated charcoal; hydrogen / ethanol / 18 h / 20 °C

4.1: chloroform / 5 h / Reflux

With sulfuric acid; palladium on activated charcoal; hydrogen; dichlorotriphenyl-λ⁴-phosphane; In ethanol; chloroform; 1,1,2,2-tetrachloroethane;

DOI:10.1080/10610278.2010.514909

Reference yield:

3-(N-ethylamino)-5-nitrobenzoic acid (90558-10-4) → C48H45N9O6 (1312807-30-9)

Guidance literature:

Multi-step reaction with 3 steps

1: dichlorotriphenyl-λ⁴-phosphane / 1,1,2,2-tetrachloroethane / 6 h / 120 °C

2: palladium on activated charcoal; hydrogen / ethanol / 18 h / 20 °C

3: chloroform / 5 h / Reflux

With palladium on activated charcoal; hydrogen; dichlorotriphenyl-λ⁴-phosphane; In ethanol; chloroform; 1,1,2,2-tetrachloroethane;

DOI:10.1080/10610278.2010.514909

upstream raw materials:

phenyl isocyanate

3-amino-5-nitro-benzoic acid

3-(N-ethylamino)-5-nitrobenzoic acid