C₂₉H₄₈N₄O₇

Base Information

Chemical Name:C₂₉H₄₈N₄O₇
CAS No.:1400436-01-2
Molecular Formula:C₂₉H₄₈N₄O₇
Molecular Weight:564.723
Hs Code.:

C<sub>29</sub>H<sub>48</sub>N<sub>4</sub>O<sub>7</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₄₈N₄O₇

Chemical Property:

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Technology Process of C₂₉H₄₈N₄O₇

There total 12 articles about C₂₉H₄₈N₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1400435-92-8
C₃₄H₅₆N₄O₉

: 1400436-01-2
C₂₉H₄₈N₄O₇

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jm3009629

Reference yield:

: 1400435-95-1
C₂₄H₃₉N₃O₆

: 1400436-01-2
C₂₉H₄₈N₄O₇

Guidance literature:: Multi-step reaction with 2 steps

1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm3009629

Reference yield:

: 1400436-10-3
C₁₄H₂₅NO₇

: 1400436-01-2
C₂₉H₄₈N₄O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 1 h / 0 - 20 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

4.2: 12 h / 20 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

6.1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

7.1: trifluoroacetic acid / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/jm3009629