(6E)-8-Benzyloxy-2,3-epoxy-2,6-dimethyl-1-octenol

Base Information

Chemical Name:(6E)-8-Benzyloxy-2,3-epoxy-2,6-dimethyl-1-octenol
CAS No.:130487-31-9
Molecular Formula:C₁₇H₂₄O₃
Molecular Weight:276.376
Hs Code.:

Synonyms:

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Chemical Property of (6E)-8-Benzyloxy-2,3-epoxy-2,6-dimethyl-1-octenol

Chemical Property:

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Technology Process of (6E)-8-Benzyloxy-2,3-epoxy-2,6-dimethyl-1-octenol

There total 3 articles about (6E)-8-Benzyloxy-2,3-epoxy-2,6-dimethyl-1-octenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 94854-66-7
(6E)-8-Benzyloxy-2,6-dimethyl-2,6-octadien-1-ol

: 130487-31-9,130551-27-8
(6E)-8-Benzyloxy-2,3-epoxy-2,6-dimethyl-1-octenol

Guidance literature:: With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; In dichloromethane; 1,2-dichloro-ethane; for 9h; Ambient temperature;
DOI:10.1246/bcsj.63.1328

Reference yield:

: 83110-40-1
((E)-6-Chloro-3,7-dimethyl-octa-2,7-dienyloxymethyl)-benzene

: 130487-31-9,130551-27-8
(6E)-8-Benzyloxy-2,3-epoxy-2,6-dimethyl-1-octenol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / sodium iodide / dimethylformamide / 12 h / 80 °C

2: 96 percent / potassium carbonate, methanol, water / 12 h / Ambient temperature

3: 97 percent / t-butyl hydroperoxide / vanadium(IV) oxide acetylacetonate / CH₂Cl₂; 1,2-dichloro-ethane / 9 h / Ambient temperature

With methanol; tert.-butylhydroperoxide; water; potassium carbonate; sodium iodide; bis(acetylacetonate)oxovanadium; In dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.63.1328

Reference yield:

: 91892-26-1
Geranyl benzyl ether

: 130487-31-9,130551-27-8
(6E)-8-Benzyloxy-2,3-epoxy-2,6-dimethyl-1-octenol

Guidance literature:: Multi-step reaction with 4 steps

1: 61percent calcium hypochlorite, dry ice / CH₂Cl₂ / 5 h

2: 90 percent / sodium iodide / dimethylformamide / 12 h / 80 °C

3: 96 percent / potassium carbonate, methanol, water / 12 h / Ambient temperature

4: 97 percent / t-butyl hydroperoxide / vanadium(IV) oxide acetylacetonate / CH₂Cl₂; 1,2-dichloro-ethane / 9 h / Ambient temperature

With methanol; tert.-butylhydroperoxide; calcium hypochlorite; Methamphetamin; water; potassium carbonate; sodium iodide; bis(acetylacetonate)oxovanadium; In dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.63.1328