vestitenone

Base Information

Chemical Name:vestitenone
CAS No.:69401-36-1
Molecular Formula:C₁₂H₁₈O
Molecular Weight:178.274
Hs Code.:

Synonyms:

Suppliers and Price of vestitenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of vestitenone

Chemical Property:

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Technology Process of vestitenone

There total 6 articles about vestitenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 138-86-3,555-08-8,8022-90-0,9003-73-0,95327-98-3
limonene.

: 69401-36-1
vestitenone

Guidance literature:: Multi-step reaction with 6 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

1.2: 2 h / 0 °C / Inert atmosphere

2.1: pyridinium chlorochromate / dichloromethane / 2 h / 0 - 20 °C

3.1: dihydrogen peroxide; potassium hydroxide / dimethyl sulfoxide; isopropyl alcohol; water / 3.5 h / 20 - 80 °C

4.1: sodium hydride / tetrahydrofuran / 0 °C / Inert atmosphere

4.2: 6.5 h / 0 - 20 °C / Inert atmosphere

5.1: sodium hydroxide; water / ethanol / 6 h / Reflux

6.1: diethyl ether / 4.5 h / 0 - 20 °C

With water; dihydrogen peroxide; sodium hydride; 9-bora-bicyclo[3.3.1]nonane; pyridinium chlorochromate; potassium hydroxide; sodium hydroxide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; dimethyl sulfoxide; isopropyl alcohol;
DOI:10.1016/j.phytochem.2017.09.017

Reference yield:

: 18479-68-0
menth-1-en-9-ol

: 69401-36-1
vestitenone

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridinium chlorochromate / dichloromethane / 2 h / 0 - 20 °C

2.1: dihydrogen peroxide; potassium hydroxide / dimethyl sulfoxide; isopropyl alcohol; water / 3.5 h / 20 - 80 °C

3.1: sodium hydride / tetrahydrofuran / 0 °C / Inert atmosphere

3.2: 6.5 h / 0 - 20 °C / Inert atmosphere

4.1: sodium hydroxide; water / ethanol / 6 h / Reflux

5.1: diethyl ether / 4.5 h / 0 - 20 °C

With water; dihydrogen peroxide; sodium hydride; pyridinium chlorochromate; potassium hydroxide; sodium hydroxide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; dimethyl sulfoxide; isopropyl alcohol;
DOI:10.1016/j.phytochem.2017.09.017

Reference yield:

: 55511-67-6
1-(4-methyl-3-cyclohexen-1-yl)ethanol

: 69401-36-1
vestitenone

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridinium chlorochromate / dichloromethane / 2 h / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran / 0 °C / Inert atmosphere

2.2: 6.5 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydroxide; water / ethanol / 6 h / Reflux

4.1: diethyl ether / 4.5 h / 0 - 20 °C

With water; sodium hydride; pyridinium chlorochromate; sodium hydroxide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
DOI:10.1016/j.phytochem.2017.09.017