7-Diphenylphosphinoyl-6-hydroxyoctanoic acid

Base Information

Chemical Name:7-Diphenylphosphinoyl-6-hydroxyoctanoic acid
CAS No.:119106-34-2
Molecular Formula:C₂₀H₂₅O₄P
Molecular Weight:360.39
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-Diphenylphosphinoyl-6-hydroxyoctanoic acid

Chemical Property:

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Technology Process of 7-Diphenylphosphinoyl-6-hydroxyoctanoic acid

There total 6 articles about 7-Diphenylphosphinoyl-6-hydroxyoctanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55983-34-1
C₂₀H₂₃OP

: 119106-34-2,119106-35-3
7-Diphenylphosphinoyl-6-hydroxyoctanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / 1.) ozone, 2.) formic acid, hydrogen peroxide 3.) diazomethane / 1.) ozone, -70 deg C, 2.) hidrogen peroxide, formic acid, 3.) diazomethane, methanol, 0 deg C

2: lithium hydroxide monohydrate / tetrahydrofuran; H₂O / 15 h / Ambient temperature

3: NaBH₄ / ethanol

With diazomethane; lithium hydroxide; sodium tetrahydroborate; formic acid; dihydrogen peroxide; ozone; In tetrahydrofuran; ethanol; water;

Reference yield:

: 1733-57-9
ethydiphenylphosphine oxide

: 119106-34-2,119106-35-3
7-Diphenylphosphinoyl-6-hydroxyoctanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / butyl lithium, copper(I) iodide / tetrahydrofuran

2: lithium hydroxide monohydrate / tetrahydrofuran; H₂O / 15 h / Ambient temperature

3: NaBH₄ / ethanol

With lithium hydroxide; sodium tetrahydroborate; copper(l) iodide; n-butyllithium; In tetrahydrofuran; ethanol; water;

Reference yield:

: 59555-99-6
1-[1-(Diphenyl-phosphinoyl)-ethyl]-cyclohexanol

: 119106-34-2,119106-35-3
7-Diphenylphosphinoyl-6-hydroxyoctanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / CF₃CO₂H

2: 62 percent / NaIO₄ / RuO₂

3: NaBH₄ / methanol

With sodium tetrahydroborate; sodium periodate; trifluoroacetic acid; ruthenium(IV) oxide; In methanol;
DOI:10.1016/S0040-4039(00)61923-8