1,3-bis(diphenylphosphino)propanedimolybdenum decacarbonyl

Base Information

Chemical Name:1,3-bis(diphenylphosphino)propanedimolybdenum decacarbonyl
CAS No.:107703-39-9
Molecular Formula:C₃₇H₂₆Mo₂O₁₀P₂
Molecular Weight:884.435
Hs Code.:

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Chemical Property of 1,3-bis(diphenylphosphino)propanedimolybdenum decacarbonyl

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Technology Process of 1,3-bis(diphenylphosphino)propanedimolybdenum decacarbonyl

There total 2 articles about 1,3-bis(diphenylphosphino)propanedimolybdenum decacarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 17594-16-0
Mo(CO)5(acetonitrile)

: 107703-39-9
1,3-bis(diphenylphosphino)propanedimolybdenum decacarbonyl

Guidance literature:: With bis(diphenylphosphino)propane; In toluene; vac. or N2 atmosphere; addn. of org. compd. to soln. of acetonitrile-complex in toluene (243 K), stirring; filtration, evapn. (vac.), dissolution (hexane/CH2Cl2 3:1), cooling (233 K), sepn., drying (vac.), removal of impurities by sublimation (room temp.); elem. anal.;

Reference yield: 42.0%

: 6737-42-4
1,3-bis-(diphenylphosphino)propane

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 107703-39-9
1,3-bis(diphenylphosphino)propanedimolybdenum decacarbonyl

: 151932-72-8
Mo(CO)5(η1-1,3-bis(diphenylphosphino)propane)

Guidance literature:: With trimethylamine-N-oxide; In tetrahydrofuran; acetonitrile; stirring Mo(CO)6 in MeCN with Me3NO*2H2O in vacuo for 20 min under Ar, dropwise transfer to a soln. of ligand in THF, stirring for 1.5 h at room temp. under Ar; removal of solvent, extn. with CH2Cl2, chromy. on silica tlc plates, elution (CH2Cl2/n-hexane), elem. anal.;
DOI:10.1016/0022-328X(93)83146-M

Reference yield:

: 107703-39-9
1,3-bis(diphenylphosphino)propanedimolybdenum decacarbonyl

: 15553-68-1
tetracarbonyl-1,3-bis(diphenylphosphino)propane-molybdenum⁽⁰⁾

Guidance literature:: With trimethylamine-N-oxide; In benzene; Refluxing of educt in benzene in presence of (CH3)3NO (N2, 24 h).;
DOI:10.1016/0022-328X(88)80553-9