3-(Dimethylphenylsilanyl)-6,11-dihydroxy-3-methyl-1,2,3,4-tetrahydrobenzanthracene-7,12-dione

Base Information

• Chemical Name: 3-(Dimethylphenylsilanyl)-6,11-dihydroxy-3-methyl-1,2,3,4-tetrahydrobenz
• Molecular Formula: C₂₇H₂₆O₄Si
• Molecular Weight: 442.587

Synonyms:

Chemical Property of 3-(Dimethylphenylsilanyl)-6,11-dihydroxy-3-methyl-1,2,3,4-tetrahydrobenz

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

There total 1 articles about 3-(Dimethylphenylsilanyl)-6,11-dihydroxy-3-methyl-1,2,3,4-tetrahydrobenzanthracene-7,12-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

5-acetoxy-2-bromo-1,4-naphthoquinone (77189-69-6) + {[3-((Z)-2-Ethoxy-2-trimethylsilanyloxy-vinyl)-1-methyl-cyclohex-3-enyl]-dimethyl-silanyl}-benzene → 6,11-Dihydroxy-3-methyl-1,2-dihydrobenzanthracene-7,12-dione + 3-(Dimethylphenylsilanyl)-6,11-dihydroxy-3-methyl-1,2,3,4-tetrahydrobenzanthracene-7,12-dione (169127-90-6) + 11-Acetoxy-3-(dimethylphenylsilanyl)-6-hydroxy-3-methyl-1,2,3,4-tetrahydrobenzanthracene-7,12-dione + 11-Acetoxy-3-(dimethylphenylsilanyl)-6-ethoxy-3-methyl-1,2,3,4-tetrahydrobenzanthracene-7,12-dione

Guidance literature:

With 3 A molecular sieve; sodium acetate; potassium carbonate; In dichloromethane; for 0.5h; Heating;

upstream raw materials:

5-acetoxy-2-bromo-1,4-naphthoquinone

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