((C₆H₅)3P)2N⁽¹⁺⁾*Co₄(CO)11COCH₃^(1-)=((C₆H₅)3P)2NCo₄(CO)11COCH₃

Base Information

Chemical Name:((C₆H₅)3P)2N⁽¹⁺⁾*Co₄(CO)11COCH₃^(1-)=((C₆H₅)3P)2NCo₄(CO)11COCH₃
CAS No.:100682-41-5
Molecular Formula:C₁₃H₃Co₄O₁₂*C₃₆H₃₀NP₂
Molecular Weight:1125.72
Hs Code.:

((C<sub>6</sub>H<sub>5</sub>)3P)2N<sup>(1+)</sup>*Co<sub>4</sub>(CO)11COCH<sub>3</sub><sup>(1-)</sup>=((C<sub>6</sub>H<sub>5</sub>)3P)2NCo<sub>4</sub>(CO)11COCH<sub>3</sub>

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Chemical Property of ((C₆H₅)3P)2N⁽¹⁺⁾*Co₄(CO)11COCH₃^(1-)=((C₆H₅)3P)2NCo₄(CO)11COCH₃

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Technology Process of ((C₆H₅)3P)2N⁽¹⁺⁾*Co₄(CO)11COCH₃^(1-)=((C₆H₅)3P)2NCo₄(CO)11COCH₃

There total 2 articles about ((C₆H₅)3P)2N⁽¹⁺⁾*Co₄(CO)11COCH₃^(1-)=((C₆H₅)3P)2NCo₄(CO)11COCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 53433-12-8
[bis(triphenylphospine)nitrogen⁽¹⁺⁾][Co(CO)4]

: [(μ3-MeC(O)OC)(CO)9Co5]

: 100682-41-5
((C₆H₅)3P)2N⁽¹⁺⁾*Co₄(CO)11COCH₃^(1-)=((C₆H₅)3P)2NCo₄(CO)11COCH₃

Guidance literature:: In tetrahydrofuran; byproducts: Co4(CO)12; a soln. of equimol. quantities of Co3(CO)9COC(O)Me and (PPN)Co(CO)4 in THF was stirred for 6 h under N2, reaction was monitored by IR spectroscopy; solvent was removed under vac., residue washed with pentane, extd. withEt2O, ext. filtered, concd., pentane was added, ppt. collected (Co4(CO)12 remained in soln.);

Reference yield: 20.0%

: 15041-50-6
tetracobaltdodecacarbonyl

: 917-54-4
methyllithium

: bis(triphenylphosphoranylidene)ammonium tetrafluoroborate

: 100682-41-5
((C₆H₅)3P)2N⁽¹⁺⁾*Co₄(CO)11COCH₃^(1-)=((C₆H₅)3P)2NCo₄(CO)11COCH₃

Guidance literature:: In diethyl ether; dichloromethane; treatment of Co-complex in Et2O with Et2O soln. of MeLi, stirring for 5min, removal of solvent, dissolution of residue in CH2Cl2 contg. (PPN)(BF4), stirring for 10 min; removal of solvent under vac., washing of residue (pentane), extn. intoEt2O, filtn., concn., pptn. by addn. of pentane;