(Z)-2-[2-Amino-3-(3,4,5-trihydroxy-phenyl)-propionylamino]-3-(3,4,5-trihydroxy-phenyl)-N-[(E)-2-(3,4,5-trihydroxy-phenyl)-vinyl]-acrylamide

Base Information

• Chemical Name: (Z)-2-[2-Amino-3-(3,4,5-trihydroxy-phenyl)-propionylamino]-3-(3,4,5-trihydroxy-phenyl)-N-[(E)-2-(3,4,5-trihydroxy-phenyl)-vinyl]-acrylamide
• CAS No.: 116050-17-0
• Molecular Formula: C₂₆H₂₅N₃O₁₁
• Molecular Weight: 555.498
• Mol file: 116050-17-0.mol

Synonyms:

Chemical Property of (Z)-2-[2-Amino-3-(3,4,5-trihydroxy-phenyl)-propionylamino]-3-(3,4,5-trihydroxy-phenyl)-N-[(E)-2-(3,4,5-trihydroxy-phenyl)-vinyl]-acrylamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z)-2-[2-Amino-3-(3,4,5-trihydroxy-phenyl)-propionylamino]-3-(3,4,5-trihydroxy-phenyl)-N-[(E)-2-(3,4,5-trihydroxy-phenyl)-vinyl]-acrylamide

There total 1 articles about (Z)-2-[2-Amino-3-(3,4,5-trihydroxy-phenyl)-propionylamino]-3-(3,4,5-trihydroxy-phenyl)-N-[(E)-2-(3,4,5-trihydroxy-phenyl)-vinyl]-acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C80H151N3O11Si9*C2HF3O2 (121072-74-0) → (Z)-2-[2-Amino-3-(3,4,5-trihydroxy-phenyl)-propionylamino]-3-(3,4,5-trihydroxy-phenyl)-N-[(E)-2-(3,4,5-trihydroxy-phenyl)-vinyl]-acrylamide (97689-87-7,116050-17-0,121209-14-1)

Guidance literature:

With pyridine; sulfure de di tert-butyle; hydrogen fluoride; for 5.5h; fractional precipitation;

DOI:10.1021/ja00198a040

Reference yield: 50.0%

acetic anhydride (108-24-7) + tunichrome B-1 (97689-87-7,116050-17-0,121209-14-1) → Acetic acid 2,6-diacetoxy-4-{(Z)-2-[(S)-2-acetylamino-3-(3,4,5-triacetoxy-phenyl)-propionylamino]-2-[(E)-2-(3,4,5-triacetoxy-phenyl)-vinylcarbamoyl]-vinyl}-phenyl ester

Guidance literature:

With pyridine; for 1h; Ambient temperature;

DOI:10.1021/ja00226a035

Reference yield: 18.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + tunichrome B-1 (97689-87-7,116050-17-0,121209-14-1) → (Z)-2-[(S)-2-Amino-3-(3,4,5-trimethoxy-phenyl)-propionylamino]-3-(3,4,5-trimethoxy-phenyl)-N-[(E)-2-(3,4,5-trimethoxy-phenyl)-vinyl]-acrylamide

Guidance literature:

In methanol; diethyl ether; for 0.75h; Ambient temperature;

DOI:10.1021/ja00226a035

upstream raw materials:

C₈₀H₁₅₁N₃O₁₁Si₉*C₂HF₃O₂

Downstream raw materials:

(+/-)-An-1 peracetate

(Z)-2-[2-Amino-3-(3,4,5-trihydroxy-phenyl)-propionylamino]-3-(3,4,5-trihydroxy-phenyl)-N-[(E)-2-(3,4,5-trihydroxy-phenyl)-vinyl]-acrylamide; compound with formic acid