dichloro(dimethylsulphoxide)tris(diphenylmethylarsine)ruthenium(II)

Base Information

Chemical Name:dichloro(dimethylsulphoxide)tris(diphenylmethylarsine)ruthenium(II)
CAS No.:89138-55-6
Molecular Formula:C₄₁H₄₅As₃Cl₂ORuS
Molecular Weight:982.614
Hs Code.:

Synonyms:

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Chemical Property of dichloro(dimethylsulphoxide)tris(diphenylmethylarsine)ruthenium(II)

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Technology Process of dichloro(dimethylsulphoxide)tris(diphenylmethylarsine)ruthenium(II)

There total 1 articles about dichloro(dimethylsulphoxide)tris(diphenylmethylarsine)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89395-66-4,75766-08-4,41290-68-0,90698-13-8,482618-33-7,194497-67-1,64376-67-6,59091-96-2,72904-47-3,61779-29-1
dichlorotetrakis(dimethyl sulfoxide)ruthenium(II)

: 945-48-2
diphenylmethylarsine

: 89138-55-6
dichloro(dimethylsulphoxide)tris(diphenylmethylarsine)ruthenium(II)

Guidance literature:: With HCl; In hydrogenchloride; ethanol; under N2 soln. of Ru complex in EtOH and concd. HCl was refluxed ca 15 min; to the hot soln. was added EtOH soln. of ligand; refluxing for ca 6h; concn., pptn. with petroleum ether, recrystn. from CH2Cl2 and Et2O; elem. anal.;
DOI:10.1016/S0277-5387(00)84383-1

Reference yield:

: 89138-55-6
dichloro(dimethylsulphoxide)tris(diphenylmethylarsine)ruthenium(II)

: 80924-72-7,55188-46-0,89164-39-6
dichloro-dicarbonyl-bis(methyldiphenylarsine)ruthenium(II)

Guidance literature:: With CO; In chloroform; stream of CO was passed through the soln. of complex until there was nofurther colour change; concn., pptn. with petroleum ether, filtration, drying; elem. anal.;
DOI:10.1016/S0277-5387(00)84383-1

Reference yield:

: 89138-55-6
dichloro(dimethylsulphoxide)tris(diphenylmethylarsine)ruthenium(II)

: 89138-63-6
hydrido(dinytrogen)(dimethylsulphoxide)tris(methyldiphenylarsine)ruthenium(II) chloride

Guidance literature:: With H₂; N₂; In N,N-dimethyl-formamide; H2 was passed through the soln. of complex and N2 was bubbled through the soln. for ca 24 h; concn., pptn. with petroleum ether; elem. anal.;
DOI:10.1016/S0277-5387(00)84383-1