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Technology Process of ((CH3)3Si)2N(CH3)2N(CH3)3SiNTaSi(C6H5)2C4H9

((CH3)3Si)2N(CH3)2N(CH3)3SiNTaSi(C6H5)2C4H9

Base Information
  • Chemical Name:((CH3)3Si)2N(CH3)2N(CH3)3SiNTaSi(C6H5)2C4H9
  • CAS No.:307352-49-4
  • Molecular Formula:C27H52N3Si4Ta
  • Molecular Weight:712.02
  • Hs Code.:
((CH<sub>3</sub>)3Si)2N(CH<sub>3</sub>)2N(CH<sub>3</sub>)3SiNTaSi(C<sub>6</sub>H<sub>5</sub>)2C<sub>4</sub>H<sub>9</sub>

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Chemical Property of ((CH3)3Si)2N(CH3)2N(CH3)3SiNTaSi(C6H5)2C4H9
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Technology Process of ((CH3)3Si)2N(CH3)2N(CH3)3SiNTaSi(C6H5)2C4H9

There total 1 articles about ((CH3)3Si)2N(CH3)2N(CH3)3SiNTaSi(C6H5)2C4H9 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

Li(thf)<SUB>3</SUB>(SitBuPh<SUB>2</SUB>)

Li(thf)3(SitBuPh2)

(Ta(μ-Cl)Cl(=NSiMe3)[N(SiMe3)2])2

(Ta(μ-Cl)Cl(=NSiMe3)[N(SiMe3)2])2

lithium dimethylamide
3585-33-9

lithium dimethylamide

((CH<sub>3</sub>)3Si)2N(CH<sub>3</sub>)2N(CH<sub>3</sub>)3SiNTaSi(C<sub>6</sub>H<sub>5</sub>)2C<sub>4</sub>H<sub>9</sub>
307352-49-4

((CH3)3Si)2N(CH3)2N(CH3)3SiNTaSi(C6H5)2C4H9

Guidance literature:
In diethyl ether; to a soln. of complex in Et2O 2 equiv of LiNMe2 was added, stirred at room temp. for 4 h, 2 equiv of Li(THF)3SiPh2Bu-t in Et2O was added dropwise with stirring, stirred at room temp. for 10 h; volatiles were removed in vac., extd. with hexanes, filtered, crystd. at -20°C; elem. anal.;
DOI:10.1021/om000503d
upstream raw materials:

lithium dimethylamide

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