(4bΞ,7S,10S,18bΞ,21S,24S)-7,14,21,28-Tetrabenzyl-10,24-di-sec-butyl-4b,7,8,10,11,18b,19,21,22,24,25,28-dodecahydrodichinolino<4,3-h:4',3'-r><1,4,7,11,14,17>hexaazacycloeicosen-6,9,12,20,23,26(5H,14H)-hexaon

Base Information

• Chemical Name: (4bΞ,7S,10S,18bΞ,21S,24S)-7,14,21,28-Tetrabenzyl-10,24-di-sec-butyl-4b,7,8,10,11,18b,19,21,22,24,25,28-dodecahydrodichinolino<4,3-h:4',3'-r><1,4,7,11,14,17>hexaazacycloeicosen-6,9,12,20,23,26(5H,14H)-hexaon
• CAS No.: 114396-57-5
• Molecular Formula: C₆₄H₆₈N₈O₆
• Molecular Weight: 1045.29

Synonyms:

Chemical Property of (4bΞ,7S,10S,18bΞ,21S,24S)-7,14,21,28-Tetrabenzyl-10,24-di-sec-butyl-4b,7,8,10,11,18b,19,21,22,24,25,28-dodecahydrodichinolino<4,3-h:4',3'-r><1,4,7,11,14,17>hexaazacycloeicosen-6,9,12,20,23,26(5H,14H)-hexaon

Chemical Property:

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Technology Process of (4bΞ,7S,10S,18bΞ,21S,24S)-7,14,21,28-Tetrabenzyl-10,24-di-sec-butyl-4b,7,8,10,11,18b,19,21,22,24,25,28-dodecahydrodichinolino<4,3-h:4',3'-r><1,4,7,11,14,17>hexaazacycloeicosen-6,9,12,20,23,26(5H,14H)-hexaon

There total 1 articles about (4bΞ,7S,10S,18bΞ,21S,24S)-7,14,21,28-Tetrabenzyl-10,24-di-sec-butyl-4b,7,8,10,11,18b,19,21,22,24,25,28-dodecahydrodichinolino<4,3-h:4',3'-r><1,4,7,11,14,17>hexaazacycloeicosen-6,9,12,20,23,26(5H,14H)-hexaon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Benzyl-3-[(1S,2S)-1-((S)-1-carbamoyl-2-phenyl-ethylcarbamoyl)-2-methyl-butylcarbamoyl]-quinolinium; bromide (114443-28-6) → (4bΞ,7S,10S,18bΞ,21S,24S)-7,14,21,28-Tetrabenzyl-10,24-di-sec-butyl-4b,7,8,10,11,18b,19,21,22,24,25,28-dodecahydrodichinolino<4,3-h:4',3'-r><1,4,7,11,14,17>hexaazacycloeicosen-6,9,12,20,23,26(5H,14H)-hexaon (114396-57-5)

Guidance literature:

With potassium hydroxide; Yield given. Multistep reaction; 1.) H₂O 2.) CH₂Cl₂; heating;

Reference yield: 53.0%

(4bΞ,7S,10S,18bΞ,21S,24S)-7,14,21,28-Tetrabenzyl-10,24-di-sec-butyl-4b,7,8,10,11,18b,19,21,22,24,25,28-dodecahydrodichinolino<4,3-h:4',3'-r><1,4,7,11,14,17>hexaazacycloeicosen-6,9,12,20,23,26(5H,14H)-hexaon (114396-57-5) → 1-Benzyl-1,4-dihydro-quinoline-3-carboxylic acid [(1S,2S)-1-((S)-1-carbamoyl-2-phenyl-ethylcarbamoyl)-2-methyl-butyl]-amide (114396-61-1)

Guidance literature:

With aluminum isopropoxide;

upstream raw materials:

1-Benzyl-3-[(1S,2S)-1-((S)-1-carbamoyl-2-phenyl-ethylcarbamoyl)-2-methyl-butylcarbamoyl]-quinolinium; bromide

Downstream raw materials:

1-Benzyl-1,4-dihydro-quinoline-3-carboxylic acid [(1S,2S)-1-((S)-1-carbamoyl-2-phenyl-ethylcarbamoyl)-2-methyl-butyl]-amide

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