3-(Benzyloxy)-4-bromobenzamide

Base Information

Chemical Name:3-(Benzyloxy)-4-bromobenzamide
CAS No.:693232-04-1
Molecular Formula:C₁₄H₁₂BrNO₂
Molecular Weight:306.159
Hs Code.:
DSSTox Substance ID:DTXSID801295377

Synonyms:3-(Benzyloxy)-4-bromobenzamide;693232-04-1;4-Bromo-3-phenylmethoxybenzamide;DTXSID801295377;4-Bromo-3-(phenylmethoxy)benzamide;A1-28984

Suppliers and Price of 3-(Benzyloxy)-4-bromobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-(Benzyloxy)-4-bromobenzamide

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:305.00514
Heavy Atom Count:18
Complexity:279

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC2=C(C=CC(=C2)C(=O)N)Br

Technology Process of 3-(Benzyloxy)-4-bromobenzamide

There total 4 articles about 3-(Benzyloxy)-4-bromobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17054-28-3
3-Benzyloxy-4-brombenzoylchlorid

: 693232-04-1
4-bromo-3-benzyoxybenzamide

Guidance literature:: With ammonium hydroxide; In 1,4-dioxane; for 0.5h;
DOI:10.1081/SCC-120028347

Reference yield:

: 17054-27-2
4-bromo-3-benzyloxybenzoic acid

: 693232-04-1
4-bromo-3-benzyoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / Heating

2: 4.0 g / NH₄OH / dioxane / 0.5 h

With ammonium hydroxide; thionyl chloride; In 1,4-dioxane;
DOI:10.1081/SCC-120028347

Reference yield:

: 14348-38-0
4-bromo-3-hydroxybenzoic acid

: 693232-04-1
4-bromo-3-benzyoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone; H₂O / 72 h / Heating

1.2: 70 percent / aq. NaOH / dioxane / Heating

2.1: thionyl chloride / Heating

3.1: 4.0 g / NH₄OH / dioxane / 0.5 h

With ammonium hydroxide; thionyl chloride; potassium carbonate; In 1,4-dioxane; water; acetone;
DOI:10.1081/SCC-120028347