2,2'-dithiobiscarbonyl>phenyl>acetamide>

Base Information

Chemical Name:2,2'-dithiobiscarbonyl>phenyl>acetamide>
CAS No.:95765-87-0
Molecular Formula:C₂₂H₂₂N₄O₈S₂
Molecular Weight:534.571
Hs Code.:

2,2'-dithiobis<N-<3-<<(carboxymethyl)amino>carbonyl>phenyl>acetamide>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2'-dithiobiscarbonyl>phenyl>acetamide>

Chemical Property:

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Technology Process of 2,2'-dithiobiscarbonyl>phenyl>acetamide>

There total 6 articles about 2,2'-dithiobiscarbonyl>phenyl>acetamide> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28547-08-2
3-<(chloroacetyl)amino>benzoic acid

: 95765-87-0
2,2'-dithiobiscarbonyl>phenyl>acetamide>

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / SOCl₂, pyridine / CHCl₃ / 2 h / 55 - 60 °C

2: 1.) NaHCO₃ / 1.) water, RT, 0.5 h, 2.) water, methanol, 16 h

3: 1.) KOH / 1.) CH₃OH, 1-5 deg C, 2.) CH₃OH, a) 0-5 deg C, 1 h, b) 40-45 deg C, 2 h

4: 89 percent / 10 percent NaOH / methanol / 2 h / 26 °C

5: 1.) I₂, piperazine hexahydrate, 2.) 1 N HCl / 1.) CH₃OH, 25 deg C, 64 h, 2.) H₂O, CH₃OH, 25 deg C, 18 h

With piperazine; pyridine; hydrogenchloride; potassium hydroxide; sodium hydroxide; thionyl chloride; iodine; sodium hydrogencarbonate; In methanol; chloroform;
DOI:10.1021/jm00145a011

Reference yield:

: 67852-69-1
3-<(chloroacetyl)amino>benzoyl chloride

: 95765-87-0
2,2'-dithiobiscarbonyl>phenyl>acetamide>

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaHCO₃ / 1.) water, RT, 0.5 h, 2.) water, methanol, 16 h

2: 1.) KOH / 1.) CH₃OH, 1-5 deg C, 2.) CH₃OH, a) 0-5 deg C, 1 h, b) 40-45 deg C, 2 h

3: 89 percent / 10 percent NaOH / methanol / 2 h / 26 °C

4: 1.) I₂, piperazine hexahydrate, 2.) 1 N HCl / 1.) CH₃OH, 25 deg C, 64 h, 2.) H₂O, CH₃OH, 25 deg C, 18 h

With piperazine; hydrogenchloride; potassium hydroxide; sodium hydroxide; iodine; sodium hydrogencarbonate; In methanol;
DOI:10.1021/jm00145a011

Reference yield:

: 67852-70-4
N-<3-<(chloroacetyl)amino>benzoyl>glycine methyl ester

: 95765-87-0
2,2'-dithiobiscarbonyl>phenyl>acetamide>

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) KOH / 1.) CH₃OH, 1-5 deg C, 2.) CH₃OH, a) 0-5 deg C, 1 h, b) 40-45 deg C, 2 h

2: 89 percent / 10 percent NaOH / methanol / 2 h / 26 °C

3: 1.) I₂, piperazine hexahydrate, 2.) 1 N HCl / 1.) CH₃OH, 25 deg C, 64 h, 2.) H₂O, CH₃OH, 25 deg C, 18 h

With piperazine; hydrogenchloride; potassium hydroxide; sodium hydroxide; iodine; In methanol;
DOI:10.1021/jm00145a011