C₃₆H₃₈Cl₃NO₁₄S₂

Base Information

Chemical Name:C₃₆H₃₈Cl₃NO₁₄S₂
CAS No.:175981-11-0
Molecular Formula:C₃₆H₃₈Cl₃NO₁₄S₂
Molecular Weight:879.187
Hs Code.:

C<sub>36</sub>H<sub>38</sub>Cl<sub>3</sub>NO<sub>14</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₃₆H₃₈Cl₃NO₁₄S₂

Chemical Property:

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Technology Process of C₃₆H₃₈Cl₃NO₁₄S₂

There total 13 articles about C₃₆H₃₈Cl₃NO₁₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108182-34-9
allyl 3,4-di-O-isopropylidene-α-L-fucopyranoside

: 175981-11-0
C₃₆H₃₈Cl₃NO₁₄S₂

Guidance literature:: Multi-step reaction with 9 steps

1: 91 percent / sodium hydride / dimethylformamide

2: 1.) HOAc / 1.) H₂O; 2.) pyridine

3: 1.) (Ph₃P)3RhCl; 2.) HCl

4: 95 percent / DBU

5: 75 percent / TMSOTf / CH₂Cl₂ / -10 °C

6: 1.) ceric ammonium nitrate / 1.) CH₃CN/H₂O; 2.) pyridine

7: 1.) p-toluenesulfonic acid, ethylmercaptan; 2.) triethylamine / 2.) -17 degC

8: 1.) Tf₂O / 1.) pyridine, -17 degC; 2.) THF, r. t.

9: 1.) tetrabutylammonium fluoride; 2.) DBU / 1.) THF, -20 degC

With hydrogenchloride; Wilkinson's catalyst; ammonium cerium(IV) nitrate; trifluoromethylsulfonic anhydride; tetrabutyl ammonium fluoride; sodium hydride; toluene-4-sulfonic acid; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; ethanethiol; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(96)00061-5

Reference yield:

: 175981-03-0
allyl 2-O-(p-methoxybenzyl)-3,4-O-isopropylidene-α-L-fucopyranoside

: 175981-11-0
C₃₆H₃₈Cl₃NO₁₄S₂

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) HOAc / 1.) H₂O; 2.) pyridine

2: 1.) (Ph₃P)3RhCl; 2.) HCl

3: 95 percent / DBU

4: 75 percent / TMSOTf / CH₂Cl₂ / -10 °C

5: 1.) ceric ammonium nitrate / 1.) CH₃CN/H₂O; 2.) pyridine

6: 1.) p-toluenesulfonic acid, ethylmercaptan; 2.) triethylamine / 2.) -17 degC

7: 1.) Tf₂O / 1.) pyridine, -17 degC; 2.) THF, r. t.

8: 1.) tetrabutylammonium fluoride; 2.) DBU / 1.) THF, -20 degC

With hydrogenchloride; Wilkinson's catalyst; ammonium cerium(IV) nitrate; trifluoromethylsulfonic anhydride; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; ethanethiol; trimethylsilyl trifluoromethanesulfonate; In dichloromethane;
DOI:10.1016/0040-4039(96)00061-5

Reference yield:

: 175980-95-7
Acetic acid (2S,3R,4R,5S,6S)-3-acetoxy-5-(4-methoxy-benzyloxy)-2-methyl-6-(2,2,2-trichloro-acetimidoyloxy)-tetrahydro-pyran-4-yl ester

: 175981-11-0
C₃₆H₃₈Cl₃NO₁₄S₂

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / TMSOTf / CH₂Cl₂ / -10 °C

2: 1.) ceric ammonium nitrate / 1.) CH₃CN/H₂O; 2.) pyridine

3: 1.) p-toluenesulfonic acid, ethylmercaptan; 2.) triethylamine / 2.) -17 degC

4: 1.) Tf₂O / 1.) pyridine, -17 degC; 2.) THF, r. t.

5: 1.) tetrabutylammonium fluoride; 2.) DBU / 1.) THF, -20 degC

With ammonium cerium(IV) nitrate; trifluoromethylsulfonic anhydride; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; ethanethiol; trimethylsilyl trifluoromethanesulfonate; In dichloromethane;
DOI:10.1016/0040-4039(96)00061-5