C₇₆H₈₆NO₂₂P

Base Information

Chemical Name:C₇₆H₈₆NO₂₂P
CAS No.:212127-47-4
Molecular Formula:C₇₆H₈₆NO₂₂P
Molecular Weight:1396.49
Hs Code.:

C<sub>76</sub>H<sub>86</sub>NO<sub>22</sub>P

Synonyms:

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Chemical Property of C₇₆H₈₆NO₂₂P

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Technology Process of C₇₆H₈₆NO₂₂P

There total 8 articles about C₇₆H₈₆NO₂₂P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34637-22-4
3-[(N-benzyloxycarbonyl)amino]propanol

: 212127-47-4
C₇₆H₈₆NO₂₂P

Guidance literature:: Multi-step reaction with 4 steps

1: 62 percent / mol. sieves 4A, MeOTf / diethyl ether; CH₂Cl₂ / -40 deg C, 30 min; 0 deg C, 12 h

2: 58 percent / ammonium cerium(IV) nitrate / toluene; ethanol; H₂O / 0.75 h

3: 1) 2-chlor-4H-1,3,2-benzodioxaphosphorin-4-one, pyridine, 2) CH₂Cl₂, acetone, 20 h

4: pivaloyl chloride, pyridine

With pyridine; 2-Chloro-4H-1,3,2-benzodioxaphosphorin-4-one; ammonium cerium(IV) nitrate; dichloromethane; 4 A molecular sieve; pivaloyl chloride; acetone; methyl trifluoromethanesulfonate; In diethyl ether; ethanol; dichloromethane; water; toluene;
DOI:10.1016/S0008-6215(97)00271-1

Reference yield:

: 5-O-allyl-1-O-benzoyl-2,3-di-O-benzyl-D-ribitol

: 212127-47-4
C₇₆H₈₆NO₂₂P

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / mol sieves 4A, NIS, TfOH / diethyl ether; 1,2-dichloro-ethane / 0.5 h / 0 °C

2: 68 percent / DABCO, RhCl(PPh₃)3, H₂O / ethanol; toluene / 0.75 h / Heating

3: pivaloyl chloride, pyridine

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; N-iodo-succinimide; trifluorormethanesulfonic acid; RhCl(PPh₃)3; 4 A molecular sieve; water; pivaloyl chloride; In diethyl ether; ethanol; 1,2-dichloro-ethane; toluene;
DOI:10.1016/S0008-6215(97)00271-1

Reference yield:

: 162466-45-7
ethyl 3,4,6-tri-O-benzyl-2-O-(p-methoxybenzyl)-1-thio-β-D-galactopyranoside

: 212127-47-4
C₇₆H₈₆NO₂₂P

Guidance literature:: Multi-step reaction with 4 steps

1: 62 percent / mol. sieves 4A, MeOTf / diethyl ether; CH₂Cl₂ / -40 deg C, 30 min; 0 deg C, 12 h

2: 58 percent / ammonium cerium(IV) nitrate / toluene; ethanol; H₂O / 0.75 h

3: 1) 2-chlor-4H-1,3,2-benzodioxaphosphorin-4-one, pyridine, 2) CH₂Cl₂, acetone, 20 h

4: pivaloyl chloride, pyridine

With pyridine; 2-Chloro-4H-1,3,2-benzodioxaphosphorin-4-one; ammonium cerium(IV) nitrate; dichloromethane; 4 A molecular sieve; pivaloyl chloride; acetone; methyl trifluoromethanesulfonate; In diethyl ether; ethanol; dichloromethane; water; toluene;
DOI:10.1016/S0008-6215(97)00271-1