(η5-cyclopentadienyl)[(2,3,12,13,14-η5)-1,4,11,15,30-pentaphenyl-1,2,4,11,15,30-hexahydro[60]fulleren-2-yl]iron

Base Information

Chemical Name:(η5-cyclopentadienyl)[(2,3,12,13,14-η5)-1,4,11,15,30-pentaphenyl-1,2,4,11,15,30-hexahydro[60]fulleren-2-yl]iron
CAS No.:863596-30-9
Molecular Formula:C₉₅H₃₀Fe
Molecular Weight:1227.13
Hs Code.:

Synonyms:

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Chemical Property of (η5-cyclopentadienyl)[(2,3,12,13,14-η5)-1,4,11,15,30-pentaphenyl-1,2,4,11,15,30-hexahydro[60]fulleren-2-yl]iron

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MSDS Files:: SDS file from LookChem

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Technology Process of (η5-cyclopentadienyl)[(2,3,12,13,14-η5)-1,4,11,15,30-pentaphenyl-1,2,4,11,15,30-hexahydro[60]fulleren-2-yl]iron

There total 1 articles about (η5-cyclopentadienyl)[(2,3,12,13,14-η5)-1,4,11,15,30-pentaphenyl-1,2,4,11,15,30-hexahydro[60]fulleren-2-yl]iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: bis(dicarbonyl(η-cyclopentadienyl)iron)

: 157791-23-6
1,4,11,15,30-pentaphenyl-2-hydro[60]fullerene

: 863596-30-9
(η5-cyclopentadienyl)[(2,3,12,13,14-η5)-1,4,11,15,30-pentaphenyl-1,2,4,11,15,30-hexahydro[60]fulleren-2-yl]iron

Guidance literature:: In benzonitrile; under inert atm. mixt. C60Ph5H and (FeCp(CO)2)2 in PhCN was heated at 180°C for 20 h; solvent was evapd., toluene was added, soln. was passed through silica pad, solvent was removed in vacuo, residue was recrystd. from CS2-hexane;
DOI:10.1021/ic050251e

Reference yield: 49.0%

: 863596-30-9
(η5-cyclopentadienyl)[(2,3,12,13,14-η5)-1,4,11,15,30-pentaphenyl-1,2,4,11,15,30-hexahydro[60]fulleren-2-yl]iron

: tris(p-bromophenylammoniumyl) hexachloroantimonate

: 863596-35-4
[Fe(η5-C60Ph5)(η5-C5H5)][SbCl6]

Guidance literature:: In tetrahydrofuran; under inert atm. to soln. Fe complex in THF ((4-BrC6H4)3N)(SbCl6) was added and stirred at 25°C for 5 h; solvent was removed in vacuo, residue was washed with water, EtOH and CHCl3, and dried in vacuo;
DOI:10.1021/ic050251e