O-ethyl phosphorochloridate

Base Information

• Chemical Name: O-ethyl phosphorochloridate
• CAS No.: 57287-75-9
• Molecular Formula: C₄H₁₀ClO₂P
• Molecular Weight: 156.549
• Mol file: 57287-75-9.mol

Synonyms:

Chemical Property of O-ethyl phosphorochloridate

Chemical Property:

Purity/Quality:

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Technology Process of O-ethyl phosphorochloridate

There total 1 articles about O-ethyl phosphorochloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(ethyloxy)ethylphosphonothioic acid (4789-36-0,5152-74-9,7776-66-1,36585-29-2) → O-ethyl ethylphosphorochloridothioate (1497-68-3,4789-37-1,13547-40-5,13547-42-7) + O-ethyl phosphorochloridate (5284-10-6,7331-88-6,57287-75-9)

Guidance literature:

With triphenyl phosphite; sulfuryl dichloride; Yield given. Multistep reaction. Yields of byproduct given; 1) CH₂Cl₂, a) -40 deg C, b) -15 deg C, 10 min., 2) benzene, hexane, -20 deg C, 10 min.;

DOI:10.1021/jo00044a035

upstream raw materials:

(ethyloxy)ethylphosphonothioic acid