Technology Process of C29H32N4O4
There total 10 articles about C29H32N4O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium carbonate / tetrahydrofuran
2: piperidine / ethanol / 3 h / Reflux
3: tetrabutyl ammonium fluoride / tetrahydrofuran
4: Dess-Martin periodane / dichloromethane
5: sodium tris(acetoxy)borohydride / dichloromethane / Molecular sieve
With
piperidine; tetrabutyl ammonium fluoride; sodium tris(acetoxy)borohydride; sodium carbonate; Dess-Martin periodane;
In
tetrahydrofuran; ethanol; dichloromethane;
DOI:10.5012/bkcs.2011.32.6.2015
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridinium chlorochromate / dichloromethane
2: piperidine / ethanol / 3 h / Reflux
3: tetrabutyl ammonium fluoride / tetrahydrofuran
4: Dess-Martin periodane / dichloromethane
5: sodium tris(acetoxy)borohydride / dichloromethane / Molecular sieve
With
piperidine; tetrabutyl ammonium fluoride; sodium tris(acetoxy)borohydride; Dess-Martin periodane; pyridinium chlorochromate;
In
tetrahydrofuran; ethanol; dichloromethane;
DOI:10.5012/bkcs.2011.32.6.2015
- Guidance literature:
-
Multi-step reaction with 4 steps
1: piperidine / ethanol / 3 h / Reflux
2: tetrabutyl ammonium fluoride / tetrahydrofuran
3: Dess-Martin periodane / dichloromethane
4: sodium tris(acetoxy)borohydride / dichloromethane / Molecular sieve
With
piperidine; tetrabutyl ammonium fluoride; sodium tris(acetoxy)borohydride; Dess-Martin periodane;
In
tetrahydrofuran; ethanol; dichloromethane;
DOI:10.5012/bkcs.2011.32.6.2015