(R)-1-(4-Bromo-phenyl)-2,2,3,3-tetrafluoro-cyclobutanecarboxylic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

Base Information

Chemical Name:(R)-1-(4-Bromo-phenyl)-2,2,3,3-tetrafluoro-cyclobutanecarboxylic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester
CAS No.:84772-59-8
Molecular Formula:C₁₉H₁₇BrF₄O₆
Molecular Weight:497.238
Hs Code.:

(R)-1-(4-Bromo-phenyl)-2,2,3,3-tetrafluoro-cyclobutanecarboxylic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

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Chemical Property of (R)-1-(4-Bromo-phenyl)-2,2,3,3-tetrafluoro-cyclobutanecarboxylic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

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Technology Process of (R)-1-(4-Bromo-phenyl)-2,2,3,3-tetrafluoro-cyclobutanecarboxylic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

There total 3 articles about (R)-1-(4-Bromo-phenyl)-2,2,3,3-tetrafluoro-cyclobutanecarboxylic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84772-58-7
1-(4-bromophenyl)-2,2,3,3-tetrafluorocyclobutane carboxylic acid

: 84772-59-8
(R)-1-(4-Bromo-phenyl)-2,2,3,3-tetrafluoro-cyclobutanecarboxylic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / Heating

2: pyridine / tetrahydrofuran

With pyridine; thionyl chloride; In tetrahydrofuran;

Reference yield:

: 5336-08-3
D-Ribono-1,4-lactone

: 84772-59-8
(R)-1-(4-Bromo-phenyl)-2,2,3,3-tetrafluoro-cyclobutanecarboxylic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 19.0 g / p-toluenesulfonic acid, acetone / 12 h

2: pyridine / tetrahydrofuran

With pyridine; toluene-4-sulfonic acid; acetone; In tetrahydrofuran;