4-methylphenyl 6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-2,3-di-O-benzoyl-4-benzyl-1-thio-α-D-galactopyranoside

Base Information Edit

Chemical Name:4-methylphenyl 6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-2,3-di-O-benzoyl-4-benzyl-1-thio-α-D-galactopyranoside
CAS No.:1602771-89-0
Molecular Formula:C₆₀H₅₉NO₂₀S
Molecular Weight:1146.19
Hs Code.:
Mol file:1602771-89-0.mol

4-methylphenyl 6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-2,3-di-O-benzoyl-4-benzyl-1-thio-α-D-galactopyranoside

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Chemical Property of 4-methylphenyl 6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-2,3-di-O-benzoyl-4-benzyl-1-thio-α-D-galactopyranoside Edit

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Technology Process of 4-methylphenyl 6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-2,3-di-O-benzoyl-4-benzyl-1-thio-α-D-galactopyranoside

There total 2 articles about 4-methylphenyl 6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-2,3-di-O-benzoyl-4-benzyl-1-thio-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 874904-93-5
C₃₄H₃₃F₃N₂O₁₄

: 942043-18-7
methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2-bromo-2,5-dideoxy-D-erythro-α-L-gluco-non-2-ulopyranosonate

: 1602771-89-0
4-methylphenyl 6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-2,3-di-O-benzoyl-4-benzyl-1-thio-α-D-galactopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; at -78 - 20 ℃; for 1h; Reagent/catalyst; Time; Inert atmosphere; Molecular sieve;
DOI:10.1002/anie.201309646

Reference yield:

: 874904-93-5
C₃₄H₃₃F₃N₂O₁₄

: 942043-18-7
methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2-bromo-2,5-dideoxy-D-erythro-α-L-gluco-non-2-ulopyranosonate

: 1602771-91-4
4-methylphenyl 6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-β-D-galacto-2-nonulopyranosylonate)-2,3-di-O-benzoyl-4-benzyl-1-thio-α-D-galactopyranoside

: 1602771-89-0
4-methylphenyl 6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-2,3-di-O-benzoyl-4-benzyl-1-thio-α-D-galactopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 1h; Overall yield = 70 %; Inert atmosphere; Molecular sieve;
DOI:10.1002/anie.201309646